Piperazinium dihydrogen phosphate, C4H12N2(H2PO4)2: Synthesis, 31P CP/MAS NMR, structural and thermal investigations

Solid State Sciences

Volumn 9, Issue 1, 2007, Pages 72-81

  Jensen, Torben R ^a   Jørgensen, Jens Erik ^a   Hazell, Rita G ^a   Jakobsen, Hans J ^a   Chevallier, Marie Agnes ^a   Jørgensen, Lene ^a   Wiedermann, Aleksandra ^a  

^a AARHUS UNIVERSITY   (Denmark)

Author keywords

31P CP MAS NMR; Crystal structure; Hydrothermal synthesis; Piperazinium phosphate; Powder diffraction; Thermal investigation

Indexed keywords

HYDROTHERMAL SYNTHESIS; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SYNTHESIS (CHEMICAL); THERMAL EFFECTS; X RAY POWDER DIFFRACTION;

HYDROTHERMAL STABILITY; PIPERAZINIUM PHOSPHATE; SOLVOTHERMAL SYNTHESES; THERMAL INVESTIGATION;

ORGANIC COMPOUNDS;

EID: 33846903846     PISSN: 12932558     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.solidstatesciences.2006.11.004     Document Type: Article

References (50)

1. Wilson S.T., Lok B.M., Messina C.A., Cannan T.R., and Flanigen E.M. J. Am. Chem. Soc. 104 (1982) 1146
2. Gier T.E., and Stucky G.D. Nature (London) 349 (1991) 508
3. Feng P., Bu X., and Stucky G.D. Nature (London) 388 (1997) 735
4. Bu X., Feng P., and Stucky G.D. Science 278 (1997) 2080
5. Cheetham A.K., Férey G., and Loiseau T. Angew. Chem., Int. Ed. Engl. 38 (1999) 3269
6. Kongshaug K.O., and Fjellvåg H. J. Solid State Chem. 175 (2003) 182
7. Sørensen M.B., Hazell R.G., Bentien A., Bond A., and Jensen T.R. J. Chem. Soc., Dalton Trans. 3 (2005) 598
8. Sørensen M.B., Hazell R.G., Pind N., and Jensen T.R. Micropor. Mesopor. Mater. 84 (2005) 144
9. Natarajan S., Neeraj S., and Rao C.N.R. Solid State Sci. 2 (2000) 87
10. Chen J., Jones R.H., Natarajan S., Hursthouse M.B., and Thomas J.M. Angew. Chem., Int. Ed. Engl. 33 (1994) 639
11. Escobal J., Pizarro J.L., Mesa J.L., Lezama L., Olazcuaga R., Arriortua M.I., and Rojo T. Chem. Mater. 12 (2000) 376
12. Riou-Cavellec M., Grenéche J.-M., Riou D., and Férey G. Chem. Mater. 10 (1998) 2434
13. Escobal J., Pizarro J.L., Mesa J.L., Arriortua M.I., and Rojo T. J. Solid State Chem. 154 (2000) 460
14. Guillou N., Gao Q., Foster P.M., Chang J., Noguès M., Park S., Férey G., and Cheetham A.K. Angew. Chem., Int. Ed. Engl. 40 (2001) 2831
15. Neeraj S., Loiseau T., Rao C.N.R., and Cheetham A.K. Solid State Sci. 6 (2004) 1169
16. Rodgers J.A., and Harrison T.A. J. Mater. Chem. 10 (2000) 2853
17. Yang G.Y., and Sevov C.S. J. Am. Chem. Soc. 121 (1999) 8389
18. Harrison W.T.A., Martin T.E., Gier T.E., and Stucky G.D. J. Mater. Chem. 2 (1992) 175
19. Harrison W.T.A., Gier T.E., Moran K.L., Nicol J.M., Eckert H., and Stucky G.D. Chem. Mater. 3 (1991) 27
20. Feng P., Bu X., and Stucky G.D. Angew. Chem., Int. Ed. Engl. 34 (1995) 1745
21. Patarin J., Marler B., and Huve L. Eur. J. Solid State Inorg. Chem. 31 (1994) 909
22. T.R. Jensen, A. Goncalves, R.G. Hazell, H.J. Jakobsen, submitted for publication.
23. Wallau M., Patarin J., Widmer I., Caullet P., Guth J.L., and Huve L. Zeolites 14 (1994) 402
24. Chavez A.V., Nenoff T.M., Hannoonman L., and Harrison W.T.A. J. Solid State Chem. 147 (1999) 584
25. Ahmadi K., Hardy A., Patarin J., and Huve L. Eur. J. Solid State Inorg. Chem. 32 (1995) 209
26. Neeraj S., Natarajan S., and Rao C.N.R. Angew. Chem., Int. Ed. Engl. 38 (1999) 3480
27. Chidambaram D., Neeraj S., Natarajan S., and Rao C.N.R. J. Solid State Chem. 147 (1999) 154
28. Choudhury A., Natarajan S., and Rao C.N.R. Inorg. Chem. 39 (2000) 4295
29. Liu W., Liu Y., Shi Z., and Pang W. J. Mater. Chem. 10 (2000) 1451
30. Neeraj S., Natarajan S., and Rao C.N.R. J. Solid State Chem. 150 (2000) 417
31. Jensen T.R., Gérentes N., Jepsen J., Hazell R.G., and Jakobsen H.J. Inorg. Chem. 44 (2005) 658
32. Rao C.N.R., Natarajan S., and Neeraj S. J. Am. Chem. Soc. 122 (2000) 2810
33. Natarajan S., Neeraj S., Choudhury A., and Rao C.N.R. Inorg. Chem. 39 (2000) 1426
34. Chippindale, et al. J. Mater. Chem. 11 (2001) 3172
35. Riou D., Loiseau Th., and Ferey G. Acta Crystallogr. C 49 (1993) 1237
36. Zima V., Lii K.-H., Nguyen N., and Ducouret A. Chem. Mater. 10 (1998) 1914
37. Sheldrick G.M. SHELXTL (1995), Siemens Analytical X-ray Systems Inc., Madison, WI
38. Altomare A., Burla M.C., Camalli M., Cascarano G.L., Giacovazzo C., Guagliardi A., Moliterni A.G.G., Polidori G., and Spagna R. J. Appl. Crystallogr. 32 (1999) 115
39. Hazell A. KRYSTAL, An integrated system of crystallographic programs (1995), Aarhus University, Denmark
40. Busing W.T., Martin K.O., and Levy H.A. ORFLS. Report ORNL-TM-305 (1962), Oak Ridge National Laboratory, Tennessee, USA
41. E. Dowty, Program ATOMS Version 5.0, Shape Software, 521 Hidden Valley Road, Kingsport, TN 37663, USA, 1997.
42. Jacobsen H.J., Daugaard P., and Langer V. J. Magn. Reson. 76 (1988) 162
43. U.S. patent 4739270, 1988.
44. Skibsted J., Nielsen N.C., Bildsøe H., and Jakobsen H.J. J. Magn. Reson. 95 (1991) 88
45. Jensen T.R., Hazell R.G., Vosegaard T., and Jakobsen H.J. Inorg. Chem. 39 (2000) 2026
46. Jensen T.R. J. Chem. Soc., Dalton Trans. 13 (1998) 2261
47. Brown I.D., and Altermatt D. Acta Crystallogr. Sect. B 41 (1985) 244
48. Grimmer A.R., Fechner E., Peter R., and Molgedey G. Chem. Phys. Lett. 77 (1981) 331
49. Grimmer A.R. Z. Chem. 24 (1984) 194
50. Turner G.L., Smith K.A., Kirkpatrick R.J., and Oldfield E. J. Magn. Reson. 70 (1986) 408