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Crystal Growth and Design

Volumn 6, Issue 12, 2006, Pages 2658-2660

One-dimensional helical chain based on decatungstate and cerium organic-inorganic hybrid material

(7) Liu, Ce a Luo, Fang a Liu, Na a Cui, Yan a Wang, Xiang a Wang, Enbo a Chen, Ji b

a NORTHEAST NORMAL UNIVERSITY (China)

b CHANGCHUN INSTITUTE OF APPLIED CHEMISTRY (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33846136067 PISSN: 15287483 EISSN: None Source Type: Journal
DOI: 10.1021/cg060610w Document Type: Article

Times cited : (41)

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- A yellow single crystal with dimensions of 0.28 x 0.24 x 0.22 mm 3 was selected for the structural analysis. Single-crystal structure determination by X-ray diffraction was performed on an R-axis RAPID IP diffractometer equipped with a normal focus, 18 kW sealed tube X-ray source (Mo Kα radiation, λ, 0.71073 Å, operating at 50 kV and 200 mA. Data processing was accomplished with the RAXWISH processing program. The structure was solved by the direct method and refined by full-matrix least squares on F2 using the SHELXL 97 software. All of the non-hydrogen atoms were refined anisotropically. The hydrogen atoms were located from difference Fourier maps. X-Ray data for 1: C23H 57CeN7O41W10, M, 3066.38, monoclinic, P2(1)/n, a, 15.217(3) Å, b, 24.475(5) Å, c, 15.889(3) Å, α, 90°, β, 93.35(3)°, γ, 9
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