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33750951285
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note
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-1, KBr): 3095(s), 2226(s), 1609(s), 1446(vs), 1416(vs), 1277(s), 1140(s), 1026(m), 1009(s), 854(vs), 843(vs), 762(s), 721(m), 567(vs), 548(m), 498(m).
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43
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33750949962
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note
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α radiation (λ = 0.71069 Å) on a Rigaku Mercury CCD diffractometer. The structure was solved by direct methods and refined with full-matrix least-squares technique using SHELXL-97 program [12]. Anisotropic thermal parameters were applied to all non-hydrogen atoms. The hydrogen atoms were generated geometrically. Crystallographic data for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Center as supplementary publication No. CCDC-613074. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: +44 1223 336 033; e-mail: deposit@ccdc.cam.ac.uk).
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