Synthesis, crystal structure and magnetic properties of a new three-dimensional porous framework: [Gd2(BDA)3(DMF)2(H2O)4] · 2DMF

Inorganic Chemistry Communications

Volumn 9, Issue 12, 2006, Pages 1223-1226

  Wu, Chuan De ^a  

^a ZHEJIANG UNIVERSITY   (China)

Author keywords

Crystal structure; Ferromagnetic interaction; Functional group; Porous framework; Tether

Indexed keywords

EID: 33750948799     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2006.07.040     Document Type: Article

References (53)

1. Oh C.M., Carpenter G.B., and Sweigart D.A. Acc. Chem. Res. 37 (2004) 1
2. Moulton B., and Zaworotko M.J. Chem. Rev. 101 (2001) 1629
3. Cotton F.A., Lin C., and Murillo C.A. Acc. Chem. Res. 34 (2001) 759
4. Eddaoudi M., Moler D.B., Li H., Chen B., Reineke T.M., O'Keeffe M., and Yaghi O.M. Acc. Chem. Res. 34 (2001) 319
5. Evans O.R., and Lin W. Acc. Chem. Res. 35 (2002) 511
6. Gade L.H. Acc. Chem. Res. 35 (2002) 575
7. Davis M.E. Nature 417 (2002) 813
8. James S.L. Chem. Soc. Rev. 32 (2003) 276
9. Janiak C. Dalton Trans. 2781 (2003) 2781
10. Rao C.N.R., Natarajan S., and Vaidhyanathan R. Angew. Chem. Int. Ed. 43 (2004) 1466
11. Yaghi O.M., O'Keeffe M., Ockwig N.W., Chae H.K., Eddaoudi M., and Kim J. Nature 423 (2003) 705
12. Suslick K.S., Bhyrappa P., Chou J.-H., Kosal M.E., Nakagaki S., Smithenry D.W., and Wilson S.R. Acc. Chem. Res. 38 (2005) 283
13. Lee S., Mallik A.B., Xu Z., Lobkovsky E.B., and Tran L. Acc. Chem. Res. 38 (2005) 251
14. Fujita M., Kwon Y.-J., Washizu S., and Ogura K. J. Am. Chem. Soc. 116 (1994) 1151
15. Seo J.S., Wand D., Lee H., Jun S.I., Oh J., Jeon Y., and Kim K. Nature 404 (2000) 982
16. Sawaki T., and Aoyama Y. J. Am. Chem. Soc. 121 (1999) 4793
17. Wu C.-D., Hu A., Zhang L., and Lin W. J. Am. Chem. Soc. 127 (2005) 8940
18. Pan L., Liu H., Lei X., Huang X., Olson D.H., Turro N.J., and Li J. Angew. Chem. Int. Ed. 42 (2003) 542
19. Noro S., Kitagawa S., Kondo M., and Seki K. Angew. Chem. Int. Ed. 39 (2000) 2081
20. Eddaoudi M., Kim J., Rosi N., Vodak D., Wachter J., O'Keeffe M., and Yaghi O.M. Science 295 (2002) 469
21. Seki K., and Mori W. J. Phys. Chem. B 106 (2002) 1380
22. Rosi N.L., Eckert J., Eddaoudi M., Vodak D.T., Kim J., O'Keeffe M., and Yaghi O.M. Science 300 (2003) 1127
23. Férey G., Latroche M., Serre C., Millange F., Loiseau T., and Percheron-Guégan A. Chem. Commun. 2976 (2003) 2976
24. Rowsell J.L.C., Millward A.R., Park K.S., and Yaghi O.M. J. Am. Chem. Soc. 126 (2004) 5666
25. Dybtsev D.N., Chun H., Yoon S.H., Kim D., and Kim K. J. Am. Chem. Soc. 126 (2004) 32
26. Bradshaw D., Prior T.J., Cussen E.J., Claridge J.B., and Rosseinsky M.J. J. Am. Chem. Soc. 126 (2004) 6106
27. Suh M.P., Ko J.W., and Choi H.J. J. Am. Chem. Soc. 124 (2002) 10976
28. Eddaoudi M., Kim J., Rosi N., Vodak D.T., Wachter J., O'Keeffe M., and Yaghi O.M. Science 295 (2002) 469
29. Rosi N.L., Eckert J., Eddaoudi M., Vodak D.T., Kim J., O'Keeffe M., and Yaghi O.M. Science 300 (2003) 1127
30. Yaghi O.M., O'Keeffe M., Ockwig N.W., Chae H.K., Eddaoudi M., and Kim J. Nature 423 (2003) 705
31. Kitaura R., Seki K., Akiyama G., and Kitagawa S. Angew. Chem. Int. Ed. 42 (2003) 428
32. Hoskins B.F., and Robson R. J. Am. Chem. Soc. 112 (1990) 1546
33. Min K.S., and Suh M.P. J. Am. Chem. Soc. 122 (2000) 6834
34. Yaghi O.M., and Li H. J. Am. Chem. Soc. 118 (1996) 295
35. Albrecht M., Lutz M., Spek A.L., and Koten G.van. Nature 406 (2000) 970
36. Real J.A., Andrés E., Muñoz M.C., Julve M., Granier T., Bousseksou A., and Varret F. Science 268 (1995) 265
37. Beauvais L.G., Shores M.P., and Long J.R. J. Am. Chem. Soc. 122 (2000) 2763
38. Liu Y.-H., Lu Y.-L., Wu H.-C., Wang J.-C., and Lu K.-L. Inorg. Chem. 41 (2002) 2592
39. Schareina T., Schick C., and Kempe R. Z. Anorg. Allg. Chem. 627 (2001) 131
40. Tynan E., Jensen P., Kruger P.E., Lees A.C., and Nieuwenhuyzen M. Dalton Trans. 1223 (2003) 1223
41. Schareina T., Schick C., Abrahams B.F., and Kempe R. Z. Anorg. Allg. Chem. 627 (2001) 1711
42. Stocco G., Guli G., Girasolo M.A., Bruno G., Nicolo F., and Scopelliti R. Acta Cryst. Sect. C 52 (1996) 829
43. Tynan E., Jensen P., Kruger P.E., and Lees A.C. Chem. Commun. 776 (2004) 776
44. Tynan E., Jensen P., Lees A.C., Moubaraki B., Murray K.S., and Kruger P.E. Cryst. Eng. Commun. 7 (2005) 90
45. Tynan E., Jensen P., Kelly N.R., Kruger P.E., Lees A.C., Moubaraki B., and Murray K.S. Dalton Trans. 3440 (2004) 3440
46. Min D., and Lee S.W. Bull. Korean Chem. Soc. 23 (2002) 948
47. -1): 1654 w, 1592 s, 1547 s, 1500 w, 1459 w, 1413 s, 1266 w, 1241 w, 1072 w, 872 w, 779 m, 730 w, 689 m, 557 w.
48. 2 = 0.0449 and S = 1.073 with 377 parameters for 5043 reflections with I > 2σ(I). The determinations of the unit cell and data collection for compound 1 were performed on a Rigaku R-AXIS RAPID. The data were collected using graphite-monochromatic MoKα radiation (λ = 0.71073 Å) at 293 K. Empirical absorption corrections were applied by using ABSCOR program. The structure was solved by direct method, and refined by full-matrix least-squares method with SHELXTL-97 program package [15]. All non-hydrogen atoms were refined anistropically. Crystallographic data (excluding structure factors) for the structure reported in this paper has been deposited with the Cambridge Crystallographic Data Center as supplementary publication no. CCDC-603053. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (Fax: +44 1223 336 033; Email: ).
49. A. L. Spek, Platon, A Multipurpose Crystallographic Tool, Utrecht University, Utrecht, The Netherlands, 2001.
50. Fisher M.E. Am. J. Phys. 32 (1964) 343
51. Costes J.-P., Clemente-Juan J.M., Dahan F., Nicodème F., and Verelst M. Angew. Chem. Int. Ed. 41 (2002) 323
52. Costes J.-P., Clemente-Juan J.M., Dahan F., and Nicodème F. Dalton Trans. 1272 (2003) 1272
53. Sheldrick G.M. Program for Structure Refinement (1997), University of Göttingen, Germany