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33750050461
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note
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An initial attempt to asymmetrically synthesize the title compound was made.
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33750057580
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note
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4. Otherwise, the two compounds have exactly the same carbon framework and molecular weight by NMR and LRMS.
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33750053452
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note
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Cyclization was extremely slow in the absence of base.
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To our knowledge, one such example was accomplished recently with a water-soluble ruthenium catalyst. See: Hong, S. H.; Grubbs, R. H. J. Am. Chem. Soc. 2006, 128, 3508-3509.
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33750042785
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note
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Published methods for the removal of the ruthenium catalyst are better suited for nonpolar compounds.
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34
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37
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33750043664
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note
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3) (see ref 8).
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38
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33750088038
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note
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3) (see ref 9).
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