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33749682326
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note
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3CN): δ = 2.83 (s, 6 H), 2.85 (s, 6 H), 4.63 (s, 2 H), 5.04 (s, 2 H), 6.95 (d, J = 7.5 Hz, 1 H), 7.03-7.05 (m, 1 H), 7.18 (d, J = 8.0 Hz, 1 H), 7.27 (d, J = 7.5 Hz, 1 H), 7.38 (t, J = 7.5 Hz, 1 H), 7.43-7.49 (m, 3 H), 7.56 (t, J = 7.0 Hz, 2 H), 7.61 (t, J = 8.0 Hz, 1 H), 7.89 (t, J = 7.5 Hz, 1 H), 8.08 (s, 1 H), 8.20 (dd, J = 6.5, J = 1.0 Hz, 1 H), 8.32 (d, J = 9.0 Hz, 1 H), 8.38 (t, J = 6.0 Hz, 2 H), 8.42 (d, J = 1.5 Hz, 1 H), 8.49 (d, J = 3.5 Hz, 1 H), 8.62 ppm (d, J = 8.0 Hz, 1 H).
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34
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1842841021
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S. A. Hilderbrand, M. H. Lim, S. J. Lippard, J. Am. Chem. Soc. 2004, 126, 4972-4978.
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36
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1542317528
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J. Kuzelka, S. Mukhopadhyay, B. Spingler, S. J. Lippard, Inorg. Chem. 2004, 43, 1751-1761.
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41
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33749676507
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note
-
CCDC 294539 and 294540 contain the supplementary crystallographic data for compounds 1 and 2, respectively. These data can be obtained free of charge from the Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/ data_request/cif.
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