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note
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2 and Fourier techniques using SHELXTL-PLUS. Absorption corrections were applied with the program SADABS. Non-hydrogen atoms were refined anisotropically. Hydrogen atoms were assigned to idealized positions and given a thermal parameter 1.2 times that of the thermal parameter of the carbon atom to which each was attached. Final residuals were R= 0.047 and wR2=0.119 for 5353 observed reflections with I > 2σ(I) and 496 variable parameters. Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-139962. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: (+ 44) 1223-336-033: e-mail: deposit@ccdc.cam. ac.uk).
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