Determination of the illicit drug gamma-hydroxybutyrate (GHB) in human saliva and beverages by 1H NMR analysis

BioFactors

Volumn 27, Issue 1-4, 2006, Pages 121-136

  Grootveld, Martin ^a   Algeo, Deborah ^a   Silwood, Christopher J L ^a   Blackburn, John C ^a   Clark, Anthony D ^a  

^a LONDON SOUTH BANK UNIVERSITY   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

4 HYDROXYBUTYRIC ACID; ILLICIT DRUG;

ADULT; ARTICLE; BEER; BEVERAGE; BODY FLUID; CALIBRATION; CAPILLARY ELECTROCHROMATOGRAPHY; CONTROLLED STUDY; GAS CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; HUMAN EXPERIMENT; HUMAN TISSUE; IMMUNOASSAY; INFRARED SPECTROSCOPY; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; NORMAL HUMAN; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; SALIVA ANALYSIS; STANDARD; VOLUNTEER;

EID: 33748935167     PISSN: 09516433     EISSN: None     Source Type: Journal    
DOI: 10.1002/biof.5520270111     Document Type: Article

References (35)

1. S.L. Chew and J.A. Meyers, Identification and quantification of gamma-hydroxybutyrate (NaGHB) by nuclear magnetic resonance spectroscopy, Journal of Forensic Science 48(2) (2003), 293-298.
2. L.A. Ciolino, Bridging the gap between GHB and GBL, Proceedings of the American Academy of Forensic Sciences Meeting 6 (2000), 44.
3. L.A. Ciolino, M.Z. Mezmer, R.D. Satzger, A.C. Machal, H.A. McCauly and A.S. Morhaus, The chemical interconversion of GHB and GBL: forensic issues and implications, Journal of Forensic Science 46(6) (2001), 1315-1323.
4. E.J. Cone, K. Kumor, L.K. Thompson and M. Sherer, Correlation of saliva cocaine levels with plasma levels and with pharmacologic effects after intravenous cocaine administration in human subjects. Journal of Analytical Toxicology 12 (1986), 200-206.
5. Substance abuse and mental health services administration, Office of Applied Substances, The Dawn Report, Club Drugs, December 2000, (updated).
6. 1H NMR analysis of GHB and GBL: further findings on the interconversion and a preliminary report on the analysis of GHB in serum and urine, Journal of Forensic Science 50(1) (2005), 81-86.
7. Drug Enforcement Administration, Gamma hydroxybutyric acid, Washington DC: Press Release March 2000.
8. I. Duarte, A. Barros, P.S. Belton, R. Righelato, M. Spraul, E. Humpfer and A.M. Gil, High resolution NMR spectroscopy and multivariate analysis for the characterisation of beer, Journal of Agricultural and Food Chemistry 50 (2002), 2475-2481.
9. D. Duchaine, Underground Steroid Handbook (II). Update: 1992, Golden CO: Mile High Publishing, 1992.
10. N. Fucci, N. de Giovanni and M. Chiraotti, Simultaneous detection of some drugs of abuse in saliva samples by SPME technique, Forensic Science International 134 (2003), 40-45.
11. A.D. Garcia, I.S. Lurie, L. Hulett and J.R. Almirral, Quantitation of gamma-hydroxybutyric acid and gamma-butyrylactone using capillary electrophoresis and high performance liquid chromatography, Proceedings of the American Acadamy of Forensic Sciences Meeting 7 (2001), 28.
12. S. Gentili, A. Torresi, R. Marsili, M. Chiarotti and T. Macchia, Simultaneous detection of amphetamine-like drugs with headspace solid-phase micro-extraction and gas chromatography-mass spectroscopy, Journal of Chromatography 780 (2002), 183-192.
13. M. Grootveld and R. Jain, Recent advances in the development of a diagnostic test for irradiated foodstuffs, Free Radical Research 6(5) (1989), 271-290.
14. M. Grootveld, R. Jain, A.W.D. Claxson, D. Naughton and D.R. Blake, The detection of irradiated foodstuffs, Trends in Food Science and Technology 1(1) (1990), 7-14.
15. M. Grootveld, A. Sheerin, M. Atherton, A.D. Millar, E.J. Lynch, D.R. Blake and D.P. Naughton, Applications of high resolution NMR analysis to the study of inflammatory joint diseases at the molecular level, in: Biomedical Applications of Spectroscopy, Advances in Spectroscopy, (Vol. 25), R.J.H. Clark and R.E. Hester, eds, John Wiley and Sons Ltd., Chichester, 1996, pp. 295-327.
16. 1H NMR analysis as a diagnostic probe for human saliva, Biochemical and Biophysical Research Communications 329 (2005), 1-5.
17. O.R. Idowu and B. Caddy, A review of the use of saliva in the forensic detection of drugs and other chemicals, Journal of the Forensic Science Society 22(2) (1982), 123-135.
18. G.N. Jenkins, The Physiology and Biochemistry of the Mouth, 4th ed., Blackwell, Oxford, 1978, 295.
19. K. Kato, M. Hillsgrove, L. Weinhold, D.A. Gorelick, W.D. Darwin and E.J. Cone, Cocaine and metabolite excretion in saliva under stimulated and non-stimulated conditions, Journal of Analytical Toxicology 17 (1993), 338-341.
20. D.A. Kidwell, J.C. Holland and S. Athanaselis, Testing for drugs of abuse in saliva and sweat, Journal of Chromatography 713 (1998), 111-135.
21. A. Krawczeniuk, The occurrence of gamma-hydroxybutyric acid (GHB) in a steroid seizure, Microgram 26(7) (1993), 160-166.
22. A. Krawczeniuk, Direct detection of gamma hydroxybutyrate (GHB): a new recreational drug via free zone capillary electrophoresis, Proceedings of the American Academy of Forensic Sciences Meeting 4 (1998), 34.
23. C. Lentner, ed., Geigy Scientific Tables, Serum, Vol. 3, 8th ed., Ciba-Geigy, Basle, 1981, 141.
24. J.C. Lindon, J.K. Nicholson and J.R. Everett, NMR spectroscopy of biofluids, Annual reports on NMR Spectroscopy 38 (1999), 1-88.
25. J.A. Morris, Extraction of GHB for FTIR analysis and a new colour test for gamma-butyrolactone (GBL), Microgram 32(8) (1999), 215.
26. The perfect crime, NEWSWEEK (2003) Feb. 3; 53.
27. J.K. Nicholson and I.D. Wilson, High resolution proton magnetic resonance spectroscopy of biological fluids, Progress in NMR Spectroscopy 21 (1989), 449-501.
28. W.N. Phillips, Anabolic Reference Guide, (6th ed.), Golden, CO: Mile High Publishing, 1991.
29. 13C nuclear magnetic resonance techniques to the characterisation of lipid oxidation products in autoxidised linoleoyl/linolenylglycerols, Lipids 34(7) (1999), 741-756.
30. 13C NMR spectroscopic analysis of human saliva, Journal of Dental Research 81(6) (2002), 422-427.
31. S. Suzuki, T. Inoue, H. Hori and S. Inayama, Analysis of methamphetamine in hair, nail, sweat and saliva by mass fragmentography, Journal of Analytical Toxicology 13 (1989), 176-178.
32. C.J. Teter and S.K. Guthrie, A comprehensive review of MDMA and GHB: two common club drugs, Pharmacotherapy 21(12) (2001), 1486-1513.
33. S.W. Toennes, S. Steinmeyer, H.-J. Maurer, M.R. Muller and G.F. Kauert, Screening of drugs of abuse in oral fluid-correlation of analysis results with serum in forensic cases. Journal of Analytical Toxicology 29(1) (2005), 22-27.
34. L.K. Thompson, D. Yousefnejad, K. Kumor, M. Sherer and E.J. Cone, Confirmation of cocaine in human saliva after intravenous use, Journal of Analytical Toxicology 11 (1987), 36-38.
35. M. Yonamine, N. Tawil, R.L. de Moraes Moreau and O. Alves Silva, Solid-phase micro-extraction-gas chromatography-mass spectroscopy of tetrahydrocannabinol, amphetamine, methamphetamine, cocaine and ethanol in saliva samples, Journal of Chromotography 789 (2003), 73-78.