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50
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33748257315
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note
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All new compounds gave satisfactory physical and analytical data.
-
-
-
-
51
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33748273156
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note
-
2O-PE. The purity of each aldehyde or ketone was checked by NMR spectroscopy.
-
-
-
-
52
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33748268566
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note
-
In the presence of 1.3 equivalent of PhIO, cis-1,2-cyclohexanedimethanol gave the γ-lactone (55% yield) and lactols (9%); 30% of the diol was recovered (as compared to Table 3, entry 2).
-
-
-
-
53
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33748263064
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note
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1H NMR data were identical with those described in the literature.
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