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31
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3643074319
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note
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See ref 7c for similar observations.
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32
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3643130490
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note
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Some residual oxidation can be observed when crude commercial NCS is used. It is completely absent when the NCS is recrystallized from toluene before use.
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-
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33
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85086290773
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note
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2 are used as cooxidants, where low yields of aldehydes are obtained. For example, see ref 7a.
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34
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3643054378
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note
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The detection level has been estimated by adding known amounts of the corresponding ketone to the crude reaction product. As little as 0.1 mol % can be detected unambiguously by GC on a OV17 capillary column.
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38
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0001628903
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Becker, H. D.; Björk, A.; Adler, E. J. Org. Chem. 1980, 45, 1596-1600.
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Adler, E.3
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