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2/MeOH) to give the amide intermediate. Amide derivative (50 mg) was dissolved in pyrrolidine (100 μL) at room temperature. After 1 h, a solution of 1 N HCl (10 mL) was added and the insoluble material was collected by filtration and dried to give de-acetylated compounds 4 or 5.
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1 were thereby obtained from the decay traces using the initial rates at 298 K.
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33746841675
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note
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Because the insolubility of compounds 4 and 5 in cyclohexane, the kinetic measurements were only performed for compounds 6 and 7 (the method is reported in Ref. 15).
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