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2 (0.030 g, 0.1 mmol) (edt = ethane-1,2-dithiolate) to give a yellow solution. After stirring at room temperature for 1 day, the solution was filtered to remove a little of the precipitate. The yellow prismatic crystals of 2 were obtained by slow diffusion of diethyl ether into the filtrate in 56% yield (based on Cu).
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28
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33746493682
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20 All non-H atoms were treated anisotropically. The positions of H atoms attached to C atoms were generated geometrically.
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