-
4
-
-
0003607021
-
-
Katritzky, A. R., Rees, C. W., Scriven, E. F. V., Eds.; Elsevier: Oxford
-
(d) Quin, L. D. In Comprehensive Heterocyclic Chemistry; Katritzky, A. R., Rees, C. W., Scriven, E. F. V., Eds.; Elsevier: Oxford, 1996; Vol. 2.
-
(1996)
Comprehensive Heterocyclic Chemistry
, vol.2
-
-
Quin, L.D.1
-
6
-
-
0242352408
-
-
(f) Hissler, M.; Dyer, P. W.; Réau, R. Coord. Chem. Rev. 2003, 244, 1.
-
(2003)
Coord. Chem. Rev.
, vol.244
, pp. 1
-
-
Hissler, M.1
Dyer, P.W.2
Réau, R.3
-
9
-
-
21144451837
-
-
(i) Hissler, M.; Lescop, C.; Réau, R. C.R. Chimie 2005, 8, 1186.
-
(2005)
C.R. Chimie
, vol.8
, pp. 1186
-
-
Hissler, M.1
Lescop, C.2
Réau, R.3
-
10
-
-
0033590710
-
-
(a) Hay, C.; LeVilain, D.; Deborde, V.; Toupet, L.; Réau, R. Chem. Commun. 1999, 345.
-
(1999)
Chem. Commun.
, pp. 345
-
-
Hay, C.1
LeVilain, D.2
Deborde, V.3
Toupet, L.4
Réau, R.5
-
11
-
-
0034657477
-
-
(b) Hay, C.; Fischmeister, C.; Hissler, M.; Toupet, L.; Réau, R. Angew. Chem., Int. Ed. 2000, 10, 1812.
-
(2000)
Angew. Chem., Int. Ed.
, vol.10
, pp. 1812
-
-
Hay, C.1
Fischmeister, C.2
Hissler, M.3
Toupet, L.4
Réau, R.5
-
12
-
-
0035476608
-
-
(c) Hay, C.; Hissler, M.; Fischmeister, C.; Rault-Berthelot, J.; Toupet, L.; Nyulaszi, L.; Réau, R. Chem-Eur. J. 2001, 7, 4222.
-
(2001)
Chem-Eur. J.
, vol.7
, pp. 4222
-
-
Hay, C.1
Hissler, M.2
Fischmeister, C.3
Rault-Berthelot, J.4
Toupet, L.5
Nyulaszi, L.6
Réau, R.7
-
13
-
-
0036247372
-
-
(d) Delaere, D.; Nguyen, M. T.; Vanquickenborne, L. G. Phys. Chem. Chem. Phys. 2002, 4, 1522.
-
(2002)
Phys. Chem. Chem. Phys.
, vol.4
, pp. 1522
-
-
Delaere, D.1
Nguyen, M.T.2
Vanquickenborne, L.G.3
-
14
-
-
0037434675
-
-
(e) Delaere, D.; Nguyen, M. T.; Vanquickenborne, L. G. J. Phys. Chem. A 2003, 107, 838.
-
(2003)
J. Phys. Chem. A
, vol.107
, pp. 838
-
-
Delaere, D.1
Nguyen, M.T.2
Vanquickenborne, L.G.3
-
15
-
-
31444434660
-
-
(f) Su, H.-C.; Fadhel, O.; Yang, C.-J.; Cho, T-Y.; Fave, C.; Hissler, M.; Wu, C.-C.; Réau, R. J. Am. Chem. Soc. 2006, 128, 983.
-
(2006)
J. Am. Chem. Soc.
, vol.128
, pp. 983
-
-
Su, H.-C.1
Fadhel, O.2
Yang, C.-J.3
Cho, T.-Y.4
Fave, C.5
Hissler, M.6
Wu, C.-C.7
Réau, R.8
-
16
-
-
0345463658
-
-
Phospholes bearing one carbonyl functional group at the 2- or 5-position have been reported. (a) Mathey, F. Tetrahedron Lett. 1973, 3255.
-
(1973)
Tetrahedron Lett.
, pp. 3255
-
-
Mathey, F.1
-
22
-
-
0034697432
-
-
(g) Niemi, T.-A.; Coe, P. L.; Till, S. J. J. Chem. Soc., Perkin Trans. 1 2000, 1519.
-
(2000)
J. Chem. Soc., Perkin Trans. 1
, pp. 1519
-
-
Niemi, T.-A.1
Coe, P.L.2
Till, S.J.3
-
23
-
-
2442657650
-
-
(h) Carmichael, D.; Klankermayer, J.; Richard, L.; Seeboth, N. Chem. Commun. 2004, 1144.
-
(2004)
Chem. Commun.
, pp. 1144
-
-
Carmichael, D.1
Klankermayer, J.2
Richard, L.3
Seeboth, N.4
-
24
-
-
0000484821
-
-
(a) Burgada, R.; Leroux, Y.; El Khoshnieh, Y. O. Tetrahedron Lett. 1981, 22, 3533.
-
(1981)
Tetrahedron Lett.
, vol.22
, pp. 3533
-
-
Burgada, R.1
Leroux, Y.2
El Khoshnieh, Y.O.3
-
25
-
-
0347336239
-
-
(b) Burgada, R.; El Khoshnieh, Y. O.; Leroux, Y. Tetrahedron 1985, 41, 1223.
-
(1985)
Tetrahedron
, vol.41
, pp. 1223
-
-
Burgada, R.1
El Khoshnieh, Y.O.2
Leroux, Y.3
-
26
-
-
37049100098
-
-
(a) Tebby, J. C.; Willetts, S. E.; Griffiths, D. V. J. Chem. Soc., Chem. Commun. 1981, 420.
-
(1981)
J. Chem. Soc., Chem. Commun.
, pp. 420
-
-
Tebby, J.C.1
Willetts, S.E.2
Griffiths, D.V.3
-
27
-
-
37049093714
-
-
(b) Caesar, J. C.; Griffiths, D. V.; Tebby, J. C.; Willetts, S. E. J. Chem. Soc., Perkin Trans. 1 1984, 1627.
-
(1984)
J. Chem. Soc., Perkin Trans. 1
, pp. 1627
-
-
Caesar, J.C.1
Griffiths, D.V.2
Tebby, J.C.3
Willetts, S.E.4
-
28
-
-
84943839284
-
-
(c) Caesar, J. C.; Griffiths, D. V.; Tebby, J. C. Phosphorus, Sulfur Silicon Relat. Elem. 1987, 29, 123.
-
(1987)
Phosphorus, Sulfur Silicon Relat. Elem.
, vol.29
, pp. 123
-
-
Caesar, J.C.1
Griffiths, D.V.2
Tebby, J.C.3
-
29
-
-
37049075784
-
-
(d) Caesar, J. C.; Griffiths, D. V.; Tebby, J. C. J. Chem. Soc., Perkin Trans. 1 1988, 175.
-
(1988)
J. Chem. Soc., Perkin Trans. 1
, pp. 175
-
-
Caesar, J.C.1
Griffiths, D.V.2
Tebby, J.C.3
-
31
-
-
33748232158
-
-
(b) Deschamps, E.; Richard, L.; Mathey, F. Angew. Chem., Int. Ed. Engl. 1994, 33, 1158.
-
(1994)
Angew. Chem., Int. Ed. Engl.
, vol.33
, pp. 1158
-
-
Deschamps, E.1
Richard, L.2
Mathey, F.3
-
32
-
-
0030849739
-
-
(a) Holand, S.; Jeanjean, M.; Mathey, F. Angew. Chem., Int. Ed. Engl. 1997, 36, 98.
-
(1997)
Angew. Chem., Int. Ed. Engl.
, vol.36
, pp. 98
-
-
Holand, S.1
Jeanjean, M.2
Mathey, F.3
-
33
-
-
0000567295
-
-
(b) Holand, S.; Maigrot, N.; Charrier, C.; Mathey, F. Organometallics 1998, 17, 2996.
-
(1998)
Organometallics
, vol.17
, pp. 2996
-
-
Holand, S.1
Maigrot, N.2
Charrier, C.3
Mathey, F.4
-
35
-
-
0242595605
-
-
(d) Melaimi, M.; Ricard, L.; Mathey, F.; Le Floch, P. Org. Lett. 2002, 4, 1245.
-
(2002)
Org. Lett.
, vol.4
, pp. 1245
-
-
Melaimi, M.1
Ricard, L.2
Mathey, F.3
Le Floch, P.4
-
36
-
-
0010357730
-
-
For example, see: (a) Ohff, A.; Pulst, S.; Lefeber, C.; Peulecke, N.; Arndt, P.; Burkalov, V. V.; Rosenthal, U. Synlett 1996, 111.
-
(1996)
Synlett
, pp. 111
-
-
Ohff, A.1
Pulst, S.2
Lefeber, C.3
Peulecke, N.4
Arndt, P.5
Burkalov, V.V.6
Rosenthal, U.7
-
38
-
-
0001565546
-
-
(c) Sato, F.; Urabe, H.; Okamoto, S. Pure Appl. Chem. 1999, 71, 1511.
-
(1999)
Pure Appl. Chem.
, vol.71
, pp. 1511
-
-
Sato, F.1
Urabe, H.2
Okamoto, S.3
-
40
-
-
0034249727
-
-
(e) Sato, F.; Urabe, H.; Okamoto, S. Chem. Rev. 2000, 100, 2835.
-
(2000)
Chem. Rev.
, vol.100
, pp. 2835
-
-
Sato, F.1
Urabe, H.2
Okamoto, S.3
-
41
-
-
18644362323
-
-
(f) Mikami, K.; Matsumoto, Y.; Shiono, T. Sci. Synth. 2003, 2, 457.
-
(2003)
Sci. Synth.
, vol.2
, pp. 457
-
-
Mikami, K.1
Matsumoto, Y.2
Shiono, T.3
-
42
-
-
0037451016
-
-
(g) Rosenthal, U.; Arndt, P.; Baumann, W.; Burlakov, V. V.; Spannenberg, A. J. Organomet. Chem. 2003, 670, 84.
-
(2003)
J. Organomet. Chem.
, vol.670
, pp. 84
-
-
Rosenthal, U.1
Arndt, P.2
Baumann, W.3
Burlakov, V.V.4
Spannenberg, A.5
-
43
-
-
33845278626
-
-
For the syntheses of 2,5-disubstituted phospholes via zirconacyclopentadienes (Fagan-Nugent method), see: (a) Pagan, P. J.; Nugent, W. A. J. Am. Chem. Soc. 1988, 110, 2310.
-
(1988)
J. Am. Chem. Soc.
, vol.110
, pp. 2310
-
-
Pagan, P.J.1
Nugent, W.A.2
-
44
-
-
84990138123
-
-
(b) Douglas, T.; Theopold, K. H. Angew. Chem., Int. Ed. Engl. 1989, 28, 1367.
-
(1989)
Angew. Chem., Int. Ed. Engl.
, vol.28
, pp. 1367
-
-
Douglas, T.1
Theopold, K.H.2
-
45
-
-
0000974285
-
-
(c) Pagan, P. J.; Nugent, W. A.; Calabrese, J. C. J. Am. Chem. Soc. 1994, 116, 1880.
-
(1994)
J. Am. Chem. Soc.
, vol.116
, pp. 1880
-
-
Pagan, P.J.1
Nugent, W.A.2
Calabrese, J.C.3
-
47
-
-
0037461412
-
-
See also ref 2
-
(e) Morisaki, Y.; Aiki, Y.; Chujo, Y. Macromolecules 2003, 36, 2594. See also ref 2.
-
(2003)
Macromolecules
, vol.36
, pp. 2594
-
-
Morisaki, Y.1
Aiki, Y.2
Chujo, Y.3
-
50
-
-
0030697490
-
-
(a) Urabe, H.; Suzuki, K.; Sato, F. J. Am. Chem. Soc. 1997, 119, 10014.
-
(1997)
J. Am. Chem. Soc.
, vol.119
, pp. 10014
-
-
Urabe, H.1
Suzuki, K.2
Sato, F.3
-
51
-
-
0030726318
-
-
(b) Urabe, H.; Takeda, T.; Hideura, D.; Sato, F. J. Am. Chem. Soc. 1997, 119, 11295.
-
(1997)
J. Am. Chem. Soc.
, vol.119
, pp. 11295
-
-
Urabe, H.1
Takeda, T.2
Hideura, D.3
Sato, F.4
-
52
-
-
0037067556
-
-
Kawasaki, T.; Saito, S.; Yamamoto, Y. J. Org. Chem. 2002, 67, 4911.
-
(2002)
J. Org. Chem.
, vol.67
, pp. 4911
-
-
Kawasaki, T.1
Saito, S.2
Yamamoto, Y.3
-
53
-
-
33746362713
-
-
note
-
In this reaction, the temperature should be kept at -50 °C during the formation of the titanacycle. Below or above this temperature, the yield of 4a decreased significantly.
-
-
-
-
54
-
-
0039827338
-
-
(a) Boymond, L.; Rottländer, M.; Cahiez, G.; Knochel P. Angew. Chem., Int. Ed. 1998, 37, 1701.
-
(1998)
Angew. Chem., Int. Ed.
, vol.37
, pp. 1701
-
-
Boymond, L.1
Rottländer, M.2
Cahiez, G.3
Knochel, P.4
-
55
-
-
9444224983
-
-
(b) Ren, H.; Krasovskiy, A.; Knochel, P. Org. Lett. 2004, 6, 4215.
-
(2004)
Org. Lett.
, vol.6
, pp. 4215
-
-
Ren, H.1
Krasovskiy, A.2
Knochel, P.3
-
56
-
-
0141645562
-
-
(c) Knochel, P.; Dohle, W.; Gommermann, N.; Kneisel, F. F.; Kopp, F.; Korn, T.; Sapountzis, I.; Vu, V. A. Angew. Chem., Int. Ed. 2003, 42, 4302.
-
(2003)
Angew. Chem., Int. Ed.
, vol.42
, pp. 4302
-
-
Knochel, P.1
Dohle, W.2
Gommermann, N.3
Kneisel, F.F.4
Kopp, F.5
Korn, T.6
Sapountzis, I.7
Vu, V.A.8
-
57
-
-
33746338373
-
-
note
-
Compounds 1a-h were prepared from the corresponding terminal-free diynes in one or two steps.
-
-
-
-
58
-
-
33746338056
-
-
note
-
w = 0.1221, R = 0.0503 (I > 2.00σ(I)), GOF = 1.16.
-
-
-
-
61
-
-
33746353807
-
-
note
-
1H NMR and mass spectrometry.
-
-
-
-
62
-
-
33746323773
-
-
note
-
Fluorescence quantum yields of 4e and 4g relative to quinine sulfate were determined to be 0.074 and 0.088%, respectively.
-
-
-
-
63
-
-
0036060925
-
-
Reáu and co-workers have extensively studied the optical properties of 2,5-diarylphosphole derivatives and disclosed the important role of an intramolecular charge-transfer interaction enforced by the presence of different types of aryl substituents, such as thienyl and pyridyl groups. See: (a) Fave, C.; Hissler, M.; Sénéchal, K.; Ledoux, I.; Zyss, J.; Réau, R. Chem. Commun. 2002, 1674.
-
(2002)
Chem. Commun.
, pp. 1674
-
-
Fave, C.1
Hissler, M.2
Sénéchal, K.3
Ledoux, I.4
Zyss, J.5
Réau, R.6
-
64
-
-
0036473453
-
-
(b) Hay, C.; Sauthier, M.; Deborde, V.; Hissler, M.; Toupet, L.; Reáu, R. J. Organomet. Chem. 2002, 643-644, 494.
-
(2002)
J. Organomet. Chem.
, vol.643-644
, pp. 494
-
-
Hay, C.1
Sauthier, M.2
Deborde, V.3
Hissler, M.4
Toupet, L.5
Reáu, R.6
-
65
-
-
33746336788
-
-
note
-
2 (382, 479); DMF (384, 485).
-
-
-
-
66
-
-
0041573625
-
-
Kamlet, M. J.; Abboud, J.-L. M.; Abraham, M. H.; Taft, R. W. J. Org. Chem. 1983, 48, 2877.
-
(1983)
J. Org. Chem.
, vol.48
, pp. 2877
-
-
Kamlet, M.J.1
Abboud, J.-L.M.2
Abraham, M.H.3
Taft, R.W.4
|