A η4-dithio-para-benzoquinone metal complex

Angewandte Chemie - International Edition

Volumn 45, Issue 23, 2006, Pages 3854-3858

  Moussa, Jamal ^a   Lev, Daniel A ^c   Boubekeur, Kamal ^a   Rager, Marie Noelle ^b   Amouri, Hani ^a  

^a CNRS   (France)

^b PSL RESEARCH UNIVERSITY   (France)

^c NORTHWESTERN UNIVERSITY SCHOOL OF LAW   (United States)

Author keywords

Coordination modes; Iridium; Quinones; Reactive intermediates; Structure elucidation

Indexed keywords

COMPLEXATION; IRIDIUM; MOLECULAR STRUCTURE; X RAY ANALYSIS;

COORDINATION MODES; QUINONES; REACTIVE INTERMEDIATES; STRUCTURE ELUCIDATION;

AROMATIC COMPOUNDS;

EID: 33746217439     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.200600414     Document Type: Article

References (28)

1. S. Patai and Z. Rappoport, The Chemistry of the Quinonoid Compounds, Wiley, New York, 2nd ed., 1988.
2. H. Bock, S. Mohmand, T. Hirabayashi, G. Maier, H. P. Reisenauer Chem. Ber. 1983, 116, 273-281.
3. R. Suzuki, K. Matsumoto, H. Kurata, M. Oda Chem. Commun. 2000, 1357-1358.
4. Y. A. Jackson, D. Rajagopal, J. Bendolph, M. Guillory, M. V. Lakshmikantham, J. Yang, M. P. Cava Org. Lett. 2003, 5, 1883-1885.
5. H. Amouri, J. Le Bras, Acc. Chem. Res. 2002, 35, 501-510, and references therein.
6. a) W. H. Hersh, R. G. Bergman J. Am. Chem. Soc. 1981, 103, 6992-6994;
7. b) A. Vigalok, D. Milstein J. Am. Chem. Soc. 1997, 119, 7873-7874;
8. c) D. B. Grotjahn, G. A. Bikzhanova, L. S. B. Collins, T. Concolino, K.-C. Lam, A. L. Rheingold J. Am. Chem. Soc. 2000, 122, 5222-5223;
9. d) Q. Zheng, J. A. Gladysz J. Am. Chem. Soc. 2005, 127, 10 508-10 509.
10. 19F NMR spectroscopy, Heyden&Son, Universities Press, Belfast, 1970, chap. 6, p. 63;
11. b) H. Amouri, M. N. Rager, F. Cagnol, J. Vaissermann Angew. Chem. 2001, 113, 3748-3750;
12. Angew. Chem. Int. Ed. 2001, 40, 3636-3638;
13. c) H. Amouri, L. Mimassi, M. N. Rager, B. E. Mann, C. Guyard-Duhayon, L. Raehm Angew. Chem. 2005, 117, 4619-4622;
14. Angew. Chem. Int. Ed. 2005, 44, 4543-4546.
15. a) J. Le Bras, H. Amouri, J. Vaissermann Organometallics 1998, 17, 1116-1121;
16. b) J. Moussa, C. Guyard-Duhayon, P. Herson, H. Amouri, M. N. Rager, A. Jutand Organometallics 2004, 23, 6231-6238.
17. -3. A single crystal of the very moisture sensitive compound 4 was selected rapidly, mounted onto a glass fiber, and transferred in a cold nitrogen gas stream. Intensity data were collected with a Bruker-Nonius Kappa-CCD with graphite-monochromated Mo-Kα radiation. Unit-cell parameters determination, data collection strategy and integration were carried out with the Nonius EVAL-14 suite of programs (A. J. M. Duisenberg, L. M. J. Kroon-Batenburg, A. M. M. Schreurs, J. Appl. Crystallogr. 2003, 36, 220). The structure was solved by direct methods using the SHELXS-86 program (G. M. Sheldrick, University of Göttingen, 1986) and refined anisotropically by full-matrix least-squares methods using the SHELXL-97 software package (G. M. Sheldrick, University of Göttingen, Germany, 1997). CCDC-293581 (4) contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from the Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/datarequest/cif.
18. a) A. Bondi J. Phys. Chem. 1964, 68, 441-451;
19. b) S.-Y. Kwon, J.-H. Cho, H.-I. Lee, U. Lee, D.-Y. Noh Inorg. Chem. Commun. 2001, 8, 510-512.
20. T. Ohashi, E. Kobayashi, T. Jinbo, J. Furukawa J. Polym. Sci. A. Polym. Chem. 1997, 35, 1621-1625.
21. M. Ratajczak-Sitarz, A. Katrusiak, Z. Kaluski, J. Garbarczyk, Acta. Cryst. C, 1987, 43, 2389-2391.
22. T. K. Venkatachalam, E. Sudbeck, F. M. Uckun J. Mol. Struct. 2005, 751, 41-54.
23. Gaussian 03, Revision C.01, M. J. Frisch, G. W. Trucks, H. B. Schlegel, G. E. Scuseria, M. A. Robb, J. R. Cheeseman, J. A. Montgomery, Jr., T. Vreven, K. N. Kudin, J. C. Burant, J. M. Millam, S. S. Iyengar, J. Tomasi, V. Barone, B. Mennucci, M. Cossi, G. Scalmani, N. Rega, G. A. Petersson, H. Nakatsuji, M. Hada, M. Ehara, K. Toyota, R. Fukuda, J. Hasegawa, M. Ishida, T. Nakajima, Y. Honda, O. Kitao, H. Nakai, M. Klene, X. Li, J. E. Knox, H. P. Hratchian, J. B. Cross, C. Adamo, J. Jaramillo, R. Gomperts, R. E. Stratmann, O. Yazyev, A. J. Austin, R. Cammi, C. Pomelli, J. W. Ochterski, P. Y. Ayala, K. Morokuma, G. A. Voth, P. Salvador, J. J. Dannenberg, V. G. Zakrzewski, S. Dapprich, A. D. Daniels, M. C. Strain, O. Farkas, D. K. Malick, A. D. Rabuck, K. Raghavachari, J. B. Foresman, J. V. Ortiz, Q. Cui, A. G. Baboul, S. Clifford, J. Cioslowski, B. B. Stefanov, G. Liu, A. Liashenko, P. Piskorz, I. Komaromi, R. L. Martin, D. J. Fox, T. Keith, M. A. Al-Laham, C. Y. Peng, A. Nanayakkara, M. Challacombe, P. M. W. Gill, B. Johnson, W. Chen, M. W. Wong, C. Gonzalez, and J. A. Pople, Gaussian, Inc., Wallingford CT, 2004.
24. a) G. N. R. Tripathi, D. M. Chipman, R. H. Schuler, D. A. Armstrong J. Phys. Chem. 1995, 99, 5264-5268;
25. b) M. Mann, J. Fabian Int. J. Quant. Chem. 1996, 60, 859-874.
26. D. A. Lev, D. B. Grotjahn, H. Amouri Organometallics 2005, 24, 4232-4240.
27. F. H. Allen, O. Kennard, D. G. Watson, L. Brammer, A. G. Orpen, R. Taylor J. Chem. Soc. Perkin Trans. 2. 1987, 12, S1-S19.
28. J. Moussa, K. Boubekeur, H. Amouri Eur. J. Inorg. Chem. 2005, 3808-3810.