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Because the conformational restriction of methyl groups would be smaller than that of methylene groups, one signal peak was observed.
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The protons on the glassware proved not to be the initiating species; whether or not the glassware for the polymerization of BTOT was silanized with a solution of 10% 1,1,1,3,3,3-hexamethyldisilazane, the results were identical.
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