Syntheses and X-ray structures of the bridging and chelating isomers of Os3(CO)10(dmpe)

Journal of Chemical Crystallography

Volumn 36, Issue 2, 2006, Pages 123-128

  Watson, William H ^a   Poola, Bhaskar ^b   Richmond, Michael G ^b  

^a TEXAS CHRISTIAN UNIVERSITY   (United States)

^b UNIVERSITY OF NORTH TEXAS   (United States)

Author keywords

1,2 bis(dimethylphosphino)ethane; Diphosphine ligands; Isomeric clusters; Triosmium clusters

Indexed keywords

EID: 33745528167     PISSN: 10741542     EISSN: None     Source Type: Journal    
DOI: 10.1007/s10870-005-9026-8     Document Type: Article

References (36)

1. Clucas, J.A.; Foster, D.F.; Harding, M.M.; Smith, A.K. J. Chem. Soc., Chem. Commun. 1984, 949.
2. Deeming, A.J.; Hardcastle, K.I.; Kabir, S.E. J. Chem. Soc. Dalton Trans. 1988, 827.
3. Colbran, S.B.; Irele, P.T.; Johnson, B.F.G.; Kaye, P.T.; Lewis, J.; Raithby, P.R. J. Chem. Soc. Dalton Trans. 1989, 2033.
4. Brown, M.P.; Dolby, P.A.; Harding, M.M.; Mathews, A.J.; Smith, A.K. J. Chem. Soc. Dalton Trans. 1993, 1671.
5. Abedin, S.M.T.; Azam, K.A.; Hursthouse, M.B.; Kabir, S.E.; Malik, K.M.A.; Mottalib, M.A.; Rosenberg, E. J. Clust. Sci. 2001, 12, 5.
6. Azam, K.A.; Hursthouse, M.B.; Islam, M.R.; Kabir, S.E.; Abdul Malik, K.M.; Miah, R.; Sudbrake, C.; Vahrenkamp, H. J. Chem. Soc. Dalton Trans. 1998, 1097.
7. Kabir, S.E.; Miah, M.A.; Sarker, N.C.; Hussain, G.M.G.; Hardcastle, K.I.; Nordlander, E.; Rosenberg, E. Organometallics 2005, 24, 3315.
8. Nicholls, J.N.; Vargas, M.D. Inorg. Synth. 1989, 26, 289.
9. Liu, Y.-C.; Yeh, W.-Y.; Lee, G.-H.; Peng, S.-M. J. Organomet. Chem. 2004, 689, 1944.
10. Drake, S.R.; Loveday, P.A. Inorg. Synth. 1990, 28, 230.
11. Shriver, D.F. The Manipulation of Air-Sensitive Compounds, McGraw-Hill: New York, 1969.
12. Saint Version 6.02, Bruker Analytical X-ray Systems, Inc. Copyright 1997-1999.
13. SHELXTL Version 5.1, Bruker Analytical X-ray Systems, Inc. Copyright 1998.
14. PLATON - A Multipurpose Crystallographic Tool, Utrecht University, Utrecht, The Netherlands, Speck, A.L. (2001).
15. For some examples of the Star of David effect in metal clusters, see: Ruff, J.K.; White, R.P. Jr.; Dahl, L.F. J. Am. Chem. Soc. 1971, 93, 2159.
16. Fumagalli, A.; Malatesta, M.C.; Vallario, M.; Ciani, G.; Moret, M.; Sironi, A. J. Clust. Sci. 2001, 12, 187.
17. Farrugia, L.J.; Mertes, P. J. Clust. Sci. 2002, 13, 199.
18. Garrou, P.E., Chem. Rev. 1981, 81, 229.
19. Deeming, A.J.; Donovan-Mtunzi, S.; Kabir, S.E. J. Organomet. Chem. 1987, 333, 253.
20. Watson, W.H.; Wu, G.; Richmond, M.G.. Organometallics 2005, 24, 5431.
21. Churchill, M.R.; DeBoer, B.G. Inorg. Chem. 1977, 16, 878.
22. Green, M.; Orpen, A.G.; Schaverien, C.J.J. Chem. Soc. Dalton Trans. 1989, 1333.
23. Bruce, M.I.; Pain, G.N.; Hughes, C.A.; Patrick, J.M.; Skelton, B.W.; White, A.H. J. Organomet. Chem. 1986, 307, 343.
24. Adams, R.D.; Tanner, J.T. Organometallics 1989, 8, 563.
25. Constable, E.C.; Johnson, B.F.G.; Khan, F.K.; Lewis, J.; Raithby, P.R.; Mikulcik, P. J. Organomet. Chem. 1991, 403, 15.
26. Biradha, K.; Hansen, V.M.; Leong, W.K.; Pomeroy, R.K.; Zaworotko, M. J. Clust. Sci. 2000, 11, 285.
27. Alex, R.F.; Einstein, F.W.B.; Jones, R.H.; Pomeroy, R.K. Inorg. Chem. 1987, 26, 3175.
28. Bruce, M.I.; Liddell, M.J.; Hughes, C.A.; Skelton, B.H.; White, A.H. J. Organomet. Chem. 1988, 347, 157.
29. Bruce, M.I.; LiddeU, M.J.; Hughes, C.A.; Patrick, J.M.; Skelton, B.H.; White, A.H. J. Organomet. Chem. 1988, 347, 181.
30. Bruce, M.I.; Liddell, M.J.; Skawkataly, O.B.; Hughes, C.A.; Skelton, B.H.; White, A.H. J. Organomet. Chem. 1988, 347, 207.
31. Lauher, J.W. J. Am. Chem. Soc. 1986, 108, 1521.
32. Orpen, A.G.; Brammer, L.; Allen, F.K.; Kennard, O.; Watson, D.G.; Taylor, R. J. Chem. Soc. Dalton Trans. 1989, SI.
33. Arif, A.M.; Hefner, J.G.; Jones, R.A.; Albright, T.A.; Kang, S.-K. J. Am. Chem. Soc. 1986, 108, 1701.
34. Schenk, W.A.; Kuemmerle, D.; Burschka, C. J. Organomet. Chem. 1988, 349, 183.
35. Don, M.-J.; Richmond, M.G.; Watson, W.H.; Kashyap, R.P. Acta Crystallogr. 1991, 47, 20.
36. Carriedo, G.A.; Sanchez, G.; Riera, V.; Bois, C.; Jeannin, Y.; Miguel, D. J. Chem. Soc. Dalton Trans. 1990, 3355.