Synthesis and X-ray crystal structures of Fe2Ru(CO) 12-n(CNBut)n and FeRu2(CO) 12-n(CNBut)n (n = 1, 2)

Journal of Cluster Science

Volumn 13, Issue 2, 2002, Pages 199-213

  Farrugia, Louis J ^a   Mertes, Peter ^a  

^a UNIVERSITY OF GLASGOW   (United Kingdom)

Author keywords

Carbonyl cluster; Disorder; Iron; Mixed metal; Ruthenium; X ray structure

Indexed keywords

CARBONYL DERIVATIVE; IRON DERIVATIVE; RUTHENIUM DERIVATIVE;

ARTICLE; CHEMICAL STRUCTURE; CRYSTAL STRUCTURE; ROENTGEN SPECTROSCOPY; SUBSTITUTION REACTION; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 0036015311     PISSN: 10407278     EISSN: None     Source Type: Journal    
DOI: 10.1023/A:1015595918064     Document Type: Article

References (40)

1. (a) D. Braga, F. Grepioni, L. J. Farrugia, and B. F. G. Johnson (1994). J. Chem. Soc., Dalton Trans., 2911 and references therein.
2. (b) L. J. Farrugia (1997). J. Chem. Soc. Dalton Trans. 1783.
3. (a) B. E. Hanson, E. C. Lisic, J. T. Petty, and G. A. Iannaconne (1986). Inorg. Chem. 25, 4062.
4. (b) S. Aime and R. Gobetto (1993). J. Cluster. Sci. 4, 1.
5. (c) H. Adams, N. A. Bailey, G. W. Bentley, and B. E. Mann (1989). J. Chem. Soc., Dalton Trans. 1831.
6. (a) B. E. Mann (1997). J. Chem. Soc. Dalton Trans. 1457.
7. (b) B. F. G. Johnson (1997). J. Chem. Soc. Dalton Trans. 1473.
8. (a) L. J. Farrugia, A. L. Gillon, D. Braga, and F. Grepioni (1999). Organometallics 18, 5022.
9. (b) D. Braga, L. J. Farrugia, A. L. Gillon, F. Grepioni, and E. Tedesco (1996). Organometallics 15, 4684.
10. L. J. Farrugia, A. M. Senior, D. Braga, F. Grepioni, A. G. Orpen, and J. G. Crossley (1996). J. Chem. Soc., Dalton Trans. 631.
11. L. J. Farrugia, D. Braga, and F. Grepioni (1999). J. Organomet. Chem. 573, 60.
12. (a) R. E. Benfield and B. F. G. Johnson (1978). J. Chem. Soc., Dalton Trans. 1554.
13. (b) B. F. G. Johnson and Y. V. Roberts (1993). Polyhedron 12, 977.
14. (c) B. F. G. Johnson and A. Bott (1990). J. Chem. Soc., Dalton Trans. 2437.
15. (d) D. Braga, C. E. Anson, A. Bott, B. F. G. Johnson, and E. Marseglia (1990). J. Chem. Soc., Dalton Trans. 3517.
16. (e) B. F. G. Johnson, Y. V. Roberts, and E. Parisini (1992). J. Chem. Soc., Dalton Trans. 2573.
17. T. Venäläinen and T. Pakkanen (1984). J. Organomet. Chem. 266, 2697.
18. (a) L. J. Farrugia, C. Rosenhahn, and S. Whitworth (1998). J. Clust. Sci. 9, 505.
19. (b) M. I. Bruce, J. G. Matisons, R. C. Wallis, J. M. Patrick, B. W. Skelton, and A. H. White (1983). J. Chem. Soc., Dalton Trans. 2365.
20. (c) M. I. Bruce, T. W. Hambley, and B. K. Nicholson (1983). J. Chem. Soc., Dalton Trans. 2385.
21. (d) J. B. Murray, B. K. Nicholson, and A. J. Whitton (1990). J. Organomet. Chem. 385, 91.
22. (a) B. F. G. Johnson, E. Parisini, and Y. V. Roberts (1993). Organometallics 12, 233.
23. (b) B. E. Mann (1999). Organometallics 11, 481.
24. (c) D. Lentz and R. Marschall (1991). Organometallics 10, 1487.
25. T. Venäläinen and T. Pakkanen (1986). J. Organomet. Chem. 316, 183.
26. D. B. W. Yawney and F. G. A. Stone (1969). J. Chem. Soc. A. 502.
27. Z. Otwinowski and W. Minor, in C. W. Carter, Jr. and R. M. Sweet (eds.), Processing of X-ray Diffraction Data Collected in Oscillation Mode, Methods in Enzymology, Vol. 276, Macromolecular Crystallography, Part A (Academic Press, 1997), pp. 307-326.
28. DENZOX-Program for processing Denzo x files, R. H. Blessing (1997). Modified for KappaCCD data, L. J. Farrugia and K. W. Muir (2001).
29. DENZOX-Program for processing Denzo x files, R. H. Blessing (1997). Modified for KappaCCD data, L. J. Farrugia and K. W. Muir (2001).
30. R. H. Blessing, (1997). J. Appl. Crystallogr. 30, 421.
31. R. H. Blessing (1995). Acta Crystallogr. A 51, 33-38.
32. P. Coppens, L. Leiserowitz, and D. Rabinovich, (1965), Acta. Cryst. 18, 1035.
33. A. Altomare, M. C. Burla, M. Camalli, G. L. Cascarano, C. Giacovazzo, A. Guagliardi, A. G. G. Moliterni, G. Polidori, and R. Spagna (1999). J. Appl. Cryst. 32, 115.
34. G. M. Sheldrick, SHELX-97 a program for crystal structure refinement; University of Göttingen, Germany, 1997, Release 97-2.
35. Tables 4.2.4.2, 4.2.6.8, and 6.1.1.4 from International Tables for Crystallography, Volume C Mathematical, Physical and Chemical Tables, Kluwer, Dordrecht, 1995.
36. L. J. Farrugia (1999). J. Appl. Crystallogr. 32, 837.
37. R. Herbst-Irmer and G. M. Sheldrick (1998). Acta Crystallogr. B 54, 443.
38. L. J. Farrugia (1997). J. Appl. Crystallogr. 30, 565.
39. J. D. Dunitz, in X-ray Analysis of the Structures of Organic Molecules (VCG: Weinheim, Germany, 1995).
40. F. L. Hirshfeld (1976). Acta Crystallogr. A 32, 239.