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33745348154
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note
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2O mixtures from 100:0 to 1:1) afforded product 12 (87 mg, 70% yield) as a yellow oil and an additional product 19 (21 mg, 23% yield).
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25
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33745350353
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note
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4 (%): C, 70.56; H, 7.61; N, 3.92. Found: C, 70.27; H, 7.43; N, 3.92.
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26
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33745377326
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note
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4 (%): C, 74.39; H, 7.80; N, 5.42. Found: C, 74.37; H, 7.77; N, 5.39.
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27
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33745362103
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note
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2O mixtures from 8:2 to 4:6) afforded product 12 (92 mg, 86% yield).
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