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Although supported by the HRMS analysis, complete characterization of the byproducts arising from the other diastereomer is complicated by the possible existence of several stereoisomers of the dimeric nitroso esters. For a relevant discussion, see: Rogic, M. M.; Demmin, T. R.; Fuhrmann, R.; Koff, F. W. J. Am. Chem. Soc. 1975, 97, 3241.
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33646441166
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note
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See Supporting Information for the preparation of the substrates.
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