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27
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33646140759
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note
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In our experimental conditions (chloroform solution, mM concentrations) the equilibrium was reached in 4 h at 263 K and in almost the mixing time of the reagents at 298 K.
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29
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33646139842
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note
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PtH (up to 70 Hz) is typical of ring-closed species rather than of linear compounds (ca. 40 Hz).
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33
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33646156823
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note
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-3, calculations and molecular graphics were carried out using PARST97 (Ref. [17]), WinGX (Ref. [18]) and ORTEP-3 for Windows (Ref. [19]) packages. CCDC - 269917 contains the supplementary crystallographic data for this paper. These data can be obtained on line free of charge from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB 2 1 EZ UK; fax +44 1223 336 033; or deposit@ccdc.cam.ac.uk.
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34
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33646125152
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Bruker, SAINT-IRIX. Bruker AXS Inc., Madison, Wisconsin, USA, 2003.
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36
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0042150179
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Sir2002: the program
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Burla M.C., Cavalli M., Carrozzini B., Cascarano G.L., Giacovazzo C., Polidori G., and Spagna R. Sir2002: the program. J. Appl. Cryst. 36 (2003) 1103
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Polidori, G.6
Spagna, R.7
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37
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33646138204
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G.M. Sheldrick, Programs for Crystal Structure Analysis (Release 97-2). Institüt für Anorganische Chemie der Universität, Tammanstrasse 4, D-3400 Göttingen, Germany, 1998.
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