메뉴 건너뛰기




Volumn 55, Issue 4, 2006, Pages 836-847

Quantifying exchange rates in chemical exchange saturation transfer agents using the saturation time and saturation power dependencies of the magnetization transfer effect on the magnetic resonance imaging signal (QUEST and QUESP): pH calibration for poly-L-lysine and a starburst dendrimer

Author keywords

CES; Chemical exchange rate; Magnetization transfer; pH; PLL; Poly L lysine; Polyamidoamine dendrimer; Saturation transfer; SPD 5

Indexed keywords

AMIDES; AMINO ACIDS; CALIBRATION; CATALYSIS; CERIUM; DENDRIMERS; FINANCE; MAGNETIC RESONANCE IMAGING; PH; PHASE LOCKED LOOPS; RATE CONSTANTS; SPECTROSCOPIC ANALYSIS;

EID: 33645772151     PISSN: 07403194     EISSN: 15222594     Source Type: Journal    
DOI: 10.1002/mrm.20818     Document Type: Article
Times cited : (285)

References (40)
  • 1
    • 0034145982 scopus 로고    scopus 로고
    • A new class of contrast agents for MRI based on proton chemical exchange dependent saturation transfer (CEST)
    • Ward K, Aletras A, Balaban R. A new class of contrast agents for MRI based on proton chemical exchange dependent saturation transfer (CEST). J Magn Reson 2000;143:79-87.
    • (2000) J Magn Reson , vol.143 , pp. 79-87
    • Ward, K.1    Aletras, A.2    Balaban, R.3
  • 2
    • 0035812395 scopus 로고    scopus 로고
    • Sensitive NMR detection of cationic-polymer-based gene delivery systems using saturation transfer via proton exchange
    • Goffeney N, Bulte JW, Duyn J, Bryant LH, Jr., van Zijl PC. Sensitive NMR detection of cationic-polymer-based gene delivery systems using saturation transfer via proton exchange. J Am Chem Soc 2001;123:8628-8629.
    • (2001) J Am Chem Soc , vol.123 , pp. 8628-8629
    • Goffeney, N.1    Bulte, J.W.2    Duyn, J.3    Bryant Jr., L.H.4    Van Zijl, P.C.5
  • 5
    • 0038101642 scopus 로고    scopus 로고
    • Sensitive CEST agents based on nucleic acid imino proton exchange: Detection of poly(rU) and of a dendrimer-poly(rU) model for nucleic acid delivery and pharmacology
    • Snoussi K, Bulte JW, Gueron M, van Zijl PC. Sensitive CEST agents based on nucleic acid imino proton exchange: detection of poly(rU) and of a dendrimer-poly(rU) model for nucleic acid delivery and pharmacology. Magn Reson Med 2003;49:998-1005.
    • (2003) Magn Reson Med , vol.49 , pp. 998-1005
    • Snoussi, K.1    Bulte, J.W.2    Gueron, M.3    Van Zijl, P.C.4
  • 6
    • 2342511016 scopus 로고    scopus 로고
    • Quantitative description of proton exchange processes between water and endogenous and exogenous agents for WEX, CEST, and APT experiments
    • Zhou J, Wilson DA, Sun PZ, Klaus JA, van Zijl PCM. Quantitative description of proton exchange processes between water and endogenous and exogenous agents for WEX, CEST, and APT experiments. Magn Reson Med 2004;51:945-952.
    • (2004) Magn Reson Med , vol.51 , pp. 945-952
    • Zhou, J.1    Wilson, D.A.2    Sun, P.Z.3    Klaus, J.A.4    Van Zijl, P.C.M.5
  • 7
    • 1642351484 scopus 로고    scopus 로고
    • Ln(III)-DOTA-MGIY complexes: A versatile series to assess the determinants of the efficacy of paramagnetic chemical exchange saturation transfer agents for magnetic resonance imaging applications
    • Terreno E, Castelli DD, Cravotto G, Milone L, Aime S. Ln(III)-DOTA-MGIY complexes: a versatile series to assess the determinants of the efficacy of paramagnetic chemical exchange saturation transfer agents for magnetic resonance imaging applications. Invest Radiol 2004;39:235-243.
    • (2004) Invest Radiol , vol.39 , pp. 235-243
    • Terreno, E.1    Castelli, D.D.2    Cravotto, G.3    Milone, L.4    Aime, S.5
  • 9
    • 0020855355 scopus 로고
    • Hydrogen exchange and structural dynamics of proteins and nucleic acids
    • Englander SW, Kallenbach NR. Hydrogen exchange and structural dynamics of proteins and nucleic acids. Q Rev Biophys 1984;16:521-655.
    • (1984) Q Rev Biophys , vol.16 , pp. 521-655
    • Englander, S.W.1    Kallenbach, N.R.2
  • 10
    • 0022396038 scopus 로고
    • Individual amide proton exchange rates in thermally unfolded basic pancreatic trypsin inhibitor
    • Roder H, Wagner G, Wuthrich K. Individual amide proton exchange rates in thermally unfolded basic pancreatic trypsin inhibitor. Biochemistry 1985;24:7407-7411.
    • (1985) Biochemistry , vol.24 , pp. 7407-7411
    • Roder, H.1    Wagner, G.2    Wuthrich, K.3
  • 11
    • 0030051552 scopus 로고    scopus 로고
    • Proton exchange rates from amino acid side chains-implications for image contrast
    • Liepinsh E, Otting G. Proton exchange rates from amino acid side chains-implications for image contrast. Magn Reson Med 1996;35:30-42.
    • (1996) Magn Reson Med , vol.35 , pp. 30-42
    • Liepinsh, E.1    Otting, G.2
  • 12
    • 0031867371 scopus 로고    scopus 로고
    • Proton NMR spectroscopy of solvent-saturable resonances: A new approach to study pH effects in situ
    • Mori S, Eleff SM, Pilatus U, Mori N, van Zijl PC. Proton NMR spectroscopy of solvent-saturable resonances: a new approach to study pH effects in situ. Magn Reson Med 1998;40:36-42.
    • (1998) Magn Reson Med , vol.40 , pp. 36-42
    • Mori, S.1    Eleff, S.M.2    Pilatus, U.3    Mori, N.4    Van Zijl, P.C.5
  • 13
    • 0033766573 scopus 로고    scopus 로고
    • Determination of pH using water protons and Chemical Exchange Dependent saturation Transfer (CEST)
    • Ward K, Balaban RS. Determination of pH Using Water Protons and Chemical Exchange Dependent Saturation Transfer (CEST). Magn Reson Med 2000;44:799-802.
    • (2000) Magn Reson Med , vol.44 , pp. 799-802
    • Ward, K.1    Balaban, R.S.2
  • 15
    • 0036204319 scopus 로고    scopus 로고
    • Paramagnetic lanthanide(III) complexes as pH-sensitive chemical exchange saturation transfer (CEST) contrast agents for MRI applications
    • Aime S, Barge A, Delli Castelli D, Fedeli F, Mortillaro A, Nielsen FU, Terreno E. Paramagnetic lanthanide(III) complexes as pH-sensitive chemical exchange saturation transfer (CEST) contrast agents for MRI applications. Magn Reson Med 2002;47:639-648.
    • (2002) Magn Reson Med , vol.47 , pp. 639-648
    • Aime, S.1    Barge, A.2    Delli Castelli, D.3    Fedeli, F.4    Mortillaro, A.5    Nielsen, F.U.6    Terreno, E.7
  • 16
    • 0029685015 scopus 로고    scopus 로고
    • Water exchange filter with improved sensitivity (WEX II) to study solvent-exchangeable protons, application to the consensus zinc finger peptide CP-1
    • Mori S, Abeygunawardana. C, Zijl Pv, Berg J. Water exchange filter with improved sensitivity (WEX II) to study solvent-exchangeable protons, application to the consensus zinc finger peptide CP-1. J Magn Reson B 1996;110:96-101.
    • (1996) J Magn Reson B , vol.110 , pp. 96-101
    • Mori, S.1    Abeygunawardana, C.2    Zijl, Pv.3    Berg, J.4
  • 17
    • 0343359244 scopus 로고
    • Investigation of exchange processes by 2-dimensional NMR-spectroscopy
    • Jeener J, Meier BH, Bachmann P, Ernst RR. Investigation of exchange processes by 2-dimensional NMR-spectroscopy. J Chem Phys 1979;71:4546-4553.
    • (1979) J Chem Phys , vol.71 , pp. 4546-4553
    • Jeener, J.1    Meier, B.H.2    Bachmann, P.3    Ernst, R.R.4
  • 18
    • 33846851242 scopus 로고
    • Study of moderately rapid chemical exchange reactions by means of nuclear magnetic double resonance
    • Forsen S, Huffman RA. Study of moderately rapid chemical exchange reactions by means of nuclear magnetic double resonance. J Chem Phys 1963;39:2892-2901.
    • (1963) J Chem Phys , vol.39 , pp. 2892-2901
    • Forsen, S.1    Huffman, R.A.2
  • 19
    • 0010957050 scopus 로고
    • Reaction rates by nuclear magnetic resonance
    • McConnell HM. Reaction rates by nuclear magnetic resonance. J Chem Phys 1958;28:430-431.
    • (1958) J Chem Phys , vol.28 , pp. 430-431
    • McConnell, H.M.1
  • 20
    • 0014945024 scopus 로고
    • Hydrogen exchange as a probe of the dynamic structure of DNA: I. General acid-base catalysis
    • McConnell BM, von Hippell PH. Hydrogen exchange as a probe of the dynamic structure of DNA: I. General acid-base catalysis. J Mol Biol 1970;50:297-316.
    • (1970) J Mol Biol , vol.50 , pp. 297-316
    • McConnell, B.M.1    Von Hippell, P.H.2
  • 21
    • 0000816766 scopus 로고    scopus 로고
    • Effects of off-resonance irradiation, cross-relaxation, and chemical exchange on steady-state magnetization and effective spin-lattice relaxation times
    • Kingsley PB, Monahan WG. Effects of off-resonance irradiation, cross-relaxation, and chemical exchange on steady-state magnetization and effective spin-lattice relaxation times. J Magn Reson 2000;143:360-375.
    • (2000) J Magn Reson , vol.143 , pp. 360-375
    • Kingsley, P.B.1    Monahan, W.G.2
  • 22
    • 16444362041 scopus 로고    scopus 로고
    • Numerical solution of the Bloch equations provides insights into the optimum design of PARACEST agents for MRI
    • Woessner DE, Zhang S, Merritt ME, Sherry AD. Numerical solution of the Bloch equations provides insights into the optimum design of PARACEST agents for MRI. Magn Reson Med 2005;53:790-799.
    • (2005) Magn Reson Med , vol.53 , pp. 790-799
    • Woessner, D.E.1    Zhang, S.2    Merritt, M.E.3    Sherry, A.D.4
  • 23
    • 36849126997 scopus 로고
    • Nuclear magnetic resonance multiplets in liquids
    • Gutowsky HS, McCall DW, Slichter CP. Nuclear magnetic resonance multiplets in liquids. J Chem Phys 1953;21:279-292.
    • (1953) J Chem Phys , vol.21 , pp. 279-292
    • Gutowsky, H.S.1    McCall, D.W.2    Slichter, C.P.3
  • 24
    • 36849121702 scopus 로고
    • Dissociation, chemical exchange, and the proton magnetic resonance in some aqueous electrolytes
    • Gutowsky HS, Saika A. Dissociation, chemical exchange, and the proton magnetic resonance in some aqueous electrolytes. J Chem Phys 1953;21:1688-1694.
    • (1953) J Chem Phys , vol.21 , pp. 1688-1694
    • Gutowsky, H.S.1    Saika, A.2
  • 25
    • 0029693096 scopus 로고    scopus 로고
    • Separation of intramolecular NOE and exchange peaks in water exchange spectroscopy using spin-echo filters
    • Mori S, Berg JM, van Zijl PCM. Separation of intramolecular NOE and exchange peaks in water exchange spectroscopy using spin-echo filters. J Biomol NMR 1996;7:77-82.
    • (1996) J Biomol NMR , vol.7 , pp. 77-82
    • Mori, S.1    Berg, J.M.2    Van Zijl, P.C.M.3
  • 26
    • 0037373411 scopus 로고    scopus 로고
    • Mechanism of magnetization transfer during on-resonance water saturation. A new approach to detect mobile proteins, peptides, and lipids
    • van Zijl PC, Zhou J, Mori N, Payen JF, Wilson D, Mori S. Mechanism of magnetization transfer during on-resonance water saturation. A new approach to detect mobile proteins, peptides, and lipids. Magn Reson Med 2003;49:440-449.
    • (2003) Magn Reson Med , vol.49 , pp. 440-449
    • Van Zijl, P.C.1    Zhou, J.2    Mori, N.3    Payen, J.F.4    Wilson, D.5    Mori, S.6
  • 27
    • 0003066693 scopus 로고
    • Solvent suppression strategies for in vivo magnetic resonance spectroscopy
    • van Zijl PCM, Moonen CT. Solvent Suppression Strategies for In Vivo Magnetic Resonance Spectroscopy. NMR Basic Princ Progr 1992;26:67-108.
    • (1992) NMR Basic Princ Progr , vol.26 , pp. 67-108
    • Van Zijl, P.C.M.1    Moonen, C.T.2
  • 29
    • 0042466426 scopus 로고    scopus 로고
    • Using the amid proton signals of intracellular proteins and petides to detect pH effects in MRI
    • Zhou J, Payen J-F, Wilson DA, Traystman RJ, van Zijl PC. Using the amid proton signals of intracellular proteins and petides to detect pH effects in MRI. Nat Med 2003;9:1085-1090.
    • (2003) Nat Med , vol.9 , pp. 1085-1090
    • Zhou, J.1    Payen, J.-F.2    Wilson, D.A.3    Traystman, R.J.4    Van Zijl, P.C.5
  • 30
    • 0034041186 scopus 로고    scopus 로고
    • Corrections for off-resonance effects and incomplete saturation in conventional (two-site) saturation-transfer kinetic measurements
    • Kingsley PB, Monahan WG. Corrections for off-resonance effects and incomplete saturation in conventional (two-site) saturation-transfer kinetic measurements. Magn Reson Med 2000;43:810-819.
    • (2000) Magn Reson Med , vol.43 , pp. 810-819
    • Kingsley, P.B.1    Monahan, W.G.2
  • 32
    • 0030744497 scopus 로고    scopus 로고
    • Correctly accounting for radiofrequency spill-over in saturation transfer experiments; application to measurement of the creatine kinase reaction rate in human forearm muscle
    • Horska A, Spencer RGS. Correctly accounting for radiofrequency spill-over in saturation transfer experiments; application to measurement of the creatine kinase reaction rate in human forearm muscle. MAGMA 1997;5:159-163.
    • (1997) MAGMA , vol.5 , pp. 159-163
    • Horska, A.1    Spencer, R.G.S.2
  • 33
    • 0032112415 scopus 로고    scopus 로고
    • Detection of proton chemical exchange between metabolites and water in biological tissues
    • Guivel-Scharen V, Sinnwell T, Wolff SD, Balaban RS. Detection of proton chemical exchange between metabolites and water in biological tissues. I Magn Reson 1998;133:36-45.
    • (1998) I Magn Reson , vol.133 , pp. 36-45
    • Guivel-Scharen, V.1    Sinnwell, T.2    Wolff, S.D.3    Balaban, R.S.4
  • 34
    • 0026951903 scopus 로고
    • Gradient-tailored excitation for single-quantum NMR spectroscopy of aqueous solutions
    • Piotto M, Saudek V, Sklenar V. Gradient-tailored excitation for single-quantum NMR spectroscopy of aqueous solutions. J Biomol NMR 1992;2:661-665.
    • (1992) J Biomol NMR , vol.2 , pp. 661-665
    • Piotto, M.1    Saudek, V.2    Sklenar, V.3
  • 35
    • 0027787894 scopus 로고
    • 2O in protein NMR. Application to sensitivity enhancements and NOE measurements
    • 2O in protein NMR. Application to sensitivity enhancements and NOE measurements. J Am Chem Soc 1993;115:12593-12594.
    • (1993) J Am Chem Soc , vol.115 , pp. 12593-12594
    • Grzesiek, S.1    Bax, A.2
  • 37
  • 38
    • 21244455698 scopus 로고    scopus 로고
    • Optimization of the irradiation power in chemical exchange dependent saturation transfer experiments
    • Sun PZ, van Zijl PCM, Zhou J. Optimization of the irradiation power in chemical exchange dependent saturation transfer experiments. J Magn Reson 2005;175:193-200.
    • (2005) J Magn Reson , vol.175 , pp. 193-200
    • Sun, P.Z.1    Van Zijl, P.C.M.2    Zhou, J.3
  • 39
    • 0031254249 scopus 로고    scopus 로고
    • Off-resonance irradiation effect in steady-state NMR saturation transfer
    • Baguet E, Roby C. Off-resonance irradiation effect in steady-state NMR saturation transfer. J Magn Reson 1997;128:149-160.
    • (1997) J Magn Reson , vol.128 , pp. 149-160
    • Baguet, E.1    Roby, C.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.