Comparison of a bioassay and a liquid chromatography-fluorescence-mass spectrometryn method for the detection of incurred enrofloxacin residues in chicken tissues

Poultry Science

Volumn 83, Issue 5, 2004, Pages 830-834

  Schneider, M J ^a   Donoghue, D J ^b  

^a EASTERN REGIONAL RESEARCH CENTER   (United States)

^b UNIVERSITY OF ARKANSAS   (United States)

Author keywords

Bioassay; Broiler tissue; Enrofloxacin; Fluoroquinolone; Liquid chromatography fluorescence mass spectrometryn

Indexed keywords

AVES; GALLUS GALLUS;

ANTIINFECTIVE AGENT; DRUG RESIDUE; ENROFLOXACIN; QUINOLONE DERIVATIVE;

ANIMAL; ARTICLE; BIOASSAY; CHEMISTRY; COMPARATIVE STUDY; DRUG EFFECT; FEMALE; FLUORESCENCE; GROWTH, DEVELOPMENT AND AGING; KLEBSIELLA PNEUMONIAE; LIQUID CHROMATOGRAPHY; MALE; MASS SPECTROMETRY; MEAT; SENSITIVITY AND SPECIFICITY; SKELETAL MUSCLE;

ANIMALS; ANTI-BACTERIAL AGENTS; BIOLOGICAL ASSAY; CHROMATOGRAPHY, LIQUID; DRUG RESIDUES; FEMALE; FLUORESCENCE; FLUOROQUINOLONES; KLEBSIELLA PNEUMONIAE; MALE; MASS SPECTROMETRY; MEAT; MUSCLE, SKELETAL; QUINOLONES; SENSITIVITY AND SPECIFICITY;

EID: 3042780317     PISSN: 00325791     EISSN: None     Source Type: Journal    
DOI: 10.1093/ps/83.5.830     Document Type: Article

References (18)

1. Barron, D., E. Jimenez-Lozano, J. Cano, and J. Barbosa. 2001. Determination of residues of enrofloxacin and its metabolite ciprofloxacin in biological materials by capillary electrophoresis. J. Chromatogr. B. Biomed. Sci. Appl. 759:73-79.
2. Beechinor, J. G., and F. J. Bloomfield. 2001. Variability in residue concentrations of tilmicosin in cattle muscle. Vet. Rec. 149:182-183.
3. Braham, R., W. D. Black, J. Claxton, and A. J. Yee. 2001. A rapid assay for detecting sulfonamides in tissues of slaughtered animals. J. Food Prot. 64:1565-1573.
4. Calderon, V., J. Gonzalez, P. Diez, and J. A. Berenquer. 1996. Evaluation of a multiple bioassay technique for determination of antibiotic residues in meat with standard solutions of antimicrobials. Food Addit. Contam. 13:13-19.
5. Code of Federal Regulations. 2003. Enrofloxacin oral solution. 21CFR520.813; and Enrofloxacin 21CFR556.228. www.gpoaccess.gov/cfr/index.html. Accessed Oct. 2003.
6. Dey, B. P., A. Thaler, and F. Gwozdz. 2003. Analysis of microbiological screen test data for antimicrobial residues in food animals. J. Environ. Sci. Health B 38:391-404.
7. Donoghue, D. J. 2003. Antibiotic residues in poultry tissues and eggs: Human health concerns? Poult. Sci. 82:618-621.
8. n for the determination of incurred enrofloxacin in whole eggs. J. AOAC Int. 86:669-674.
9. Garcia, M. A., C. Solans, E. Hernandez, M. Puig, and M. A. Bregante. 2001. Simultaneous determination of enrofloxacin and its primary metabolite, ciprofloxaein, in chicken tissues. Chromatographia 54:191-194.
10. Horie, M., K. Saito, N. Nose, and H. Nakazawa. 1994. Simultaneous determination of benofloxacin, danofloxacin, enrofloxacin and ofloxacin in chicken tissues by high performance liquid chromatography. J. Chromatogr. B. Biomed. Appl. 653:69-76.
11. Horstkotter, C., E. Jimenez-Lozano, D. Barron, J. Barbosa, and G. Blaschke. 2002. Determination of residues of enrofloxacin and its metabolite ciprofloxaein in chicken muscle by capillary electrophoresis using laser-induced fluorescence detection. Electrophoresis 23:3078-3083.
12. Resurreccion, A. V. A., and F. C. F. Galvez. 1999. Will consumers buy irradiated beef? Food Technol. 53:52-55.
13. Rose, M. D., J. Bygrave, and G. W. F. Stubbings. 1998. Extension of multi-residue methodology to include the determination of quinolones in food. Analyst 123:2789-2796.
14. SAS Institute. 1994. SAS User's Guide. 4th ed. SAS Institute, Cary, NC.
15. Schneider, M. J., and D. J. Donoghue. 2002. Multiresidue analysis of fluoroquinolone antibiotics in chicken tissue using liquid chromatography- fluorescence-multiple mass spectrometry. J. Chromatogr. B. Anal. Technol. Biomed. Life Sci. 780:83-92.
16. Waggoner, T. B., and M. C. Bowman. 1987. Spectrofluorometric determination of BAY Vp 2674 residues in poultry tissues. J. AOAC Int. 70:813-818.
17. World Health Organization. 1998. Use of quinolones in food animals and potential impact on human health. WHO, Geneva, Switzerland.
18. Yorke, J. C., and P. Froc. 2000. Quantitation of nine quinolones in chicken tissues by high-performance liquid chromatography with fluorescence detection. J. Chromatogr. A 882:63-77.