Synthesis and structural characterization of silanethiolato complexes having tert-butyldimethylsilyl and trimethylsilyl groups

Dalton Transactions

Volumn , Issue 10, 2004, Pages 1618-1625

  Komuro, Takashi ^a   Matsuo, Tsukasa ^b   Kawaguchi, Hiroyuki ^b   Tatsumi, Kazuyuki ^a  

^a NAGOYA UNIVERSITY   (Japan)

^b INSTITUTE FOR MOLECULAR SCIENCE   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

COOLING; CRYSTALLOGRAPHY; ELECTRONIC PROPERTIES; INFRARED SPECTROGRAPHS; IRON; LITHIUM; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SILANES; SILICON; SINGLE CRYSTALS; SULFUR; THERMAL EFFECTS; X RAY DIFFRACTION;

BUTYLDIMETHYLSILYL; CYCLOTRISILATHIANE; SILANETHIOLATO COMPLEXES; TRIMETHYSILYL GROUPS;

AROMATIC COMPOUNDS;

EID: 3042724720     PISSN: 14779226     EISSN: None     Source Type: Journal    
DOI: 10.1039/b316567a     Document Type: Article

References (66)

1. (a) D. T. T. Tran, L. M. C. Beltran, C. M. Kowalohuk, N. R. Trefiak, N. J. Taylor and J. F. Corrigan, Inorg. Chem. 2002, 41, 5963-5698;
2. (b) D. T. T. Tran, N. J. Taylor and J. F. Corrigan, Angew. Chem., Int. Ed., 2000, 39, 935-937;
3. (c) M. W. DeGroot, N. J. Taylor and J. F. Corrigan, J. Am. Chem. Soc., 2003, 125, 864-865.
4. (a) H.-C. Liang and P. A. Shapley, Orgcmometallics, 1996, 15, 1331-1333;
5. (b) P. A. Shapley, H.-C. Liang and N. C. Dopke, Orgcmometallics, 2001, 20, 4700-4704.
6. (a) L. Cai and R. H. Holm, J. Am. Chem. Soc., 1994, 116, 7177-7188;
7. (i) C. Zhou, L. Cai and R. H. Holm, Inorg. Chem., 1996, 35, 2767-2772.
8. T. Komuro, T. Matsuo, H. Kawaguchi and K. Tatsumi, Chem. Commun., 2002, 988-989.
9. T. Komuro, T. Matsuo, H. Kawaguchi and K. Tatsumi, Angew. Chem., Int. Ed., 2003, 42, 465-468.
10. A. E. Pierce, Silylation of Organic Compounds, Pierce Chemical Co., Rockford, IL 1968; L. H. Sommer, Stereochemistry, Mechanism and Silicon, McGraw-Hill, New York, 1965.
11. A. E. Pierce, Silylation of Organic Compounds, Pierce Chemical Co., Rockford, IL 1968; L. H. Sommer, Stereochemistry, Mechanism and Silicon, McGraw-Hill, New York, 1965.
12. (a) E. J. Corey and A. Venkateswarlu, J. Am. Chem. Soc., 1972, 94, 6190-6191;
13. (b) G. Stork and P. F. Hudrlik, J. Am. Chem. Soc., 1968, 90, 4462-4464;
14. (c) G. Stork and P. F. Hudrlik, J. Am. Chem. Soc., 1968, 90, 4462-4465;
15. (d) C. Rücker, Chem. Rev., 1995, 95, 1009-1064.
16. T. Komuro, H. Kawaguchi and K. Tatsumi, Inorg. Chem., 2002, 41, 5083-5090.
17. (a) D. T. T. Tran and J. F. Corrigan, Organometallics, 2000, 19, 5202-5208;
18. (b) A. I. Wallbank and J. F. Corrigan, Can. J. Chem., 2002, 80, 1592-1599;
19. (c) S.-B. Yu, Polyhedron, 1992, 11, 2115-2117.
20. (a) I. Kovács, F. Belanger-Gariepy and A. Shaver, Inorg. Chem., 2003, 42, 2988-2991;
21. (b) I. Kovács, A.-M. Lebuis and A. Shaver, Organometallics, 2001, 20, 35-41;
22. (c) I. Kovács, C. Pearson and A. Shaver, J. Organomet. Chem., 2000, 596, 193-203.
23. (a) B. Becker, K. Radacki and W. Wojnowski, J. Organomet. Chem., 1996, 521, 39-49;
24. (b) W. Wojnowski, B. Becker, L. Waltz, K. Peters, E.-M. Peters and H. G. von Schnering, Polyhedron, 1992, 11, 607-612;
25. (c) B. Becker, W. Wojnowski, K. Peters, E.-M. Peters and H. G. von Schnering, Polyhedron, 1992, 11, 613-616;
26. (d) B. Becker, K. Radacki, A. Konitz and W. Wojnowski, Z. Anorg. Allg. Chem., 1995, 621, 904-908;
27. (e) B. Becker, W. Wojnowski, K. Peters, E.-M. Peters and H. G. von Schnering, Inorg. Chim. Acta, 1993, 214, 9-11;
28. (f) B. Becker, A. Zalewska, A. Konitz and W. Wojnowski, Polyhedron, 2001, 20, 2567-2576.
29. B. Becker, W. Wojnowski, K. Peters, E.-M. Peters and von Schnering, Polyhedron, 1990, 9, 1659-1666.
30. (a) J. Chojnacki, B. Becker, A. Konitz, M. J. Potrzebowski and W. Wojnowski, J. Chem. Soc., Dalton Trans., 1999, 3063-3068;
31. (b) W. Wojnowski, M. Wojnowski, K. Peters, E.-M. Peters and H. G. von Schnering, Z. Anorg. Allg. Chem., 1985, 530, 79-88;
32. (c) W. Wojnowski, B. Becker, J. Sassmannshausen, E.-M. Peters, K. Peters and H. G. von Schnering, Z Anorg. Allg. Chem., 1994, 620, 1417-1421.
33. A. Bauer, W. Schneider, K. Angermaier, A. Schier and H. Schmidbaur, Inorg. Chim. Acta, 1996, 251, 249-253.
34. D. M. Giolando, T. B. Rauchfuss and G. M. Clark, Inorg. Chem., 1987, 26, 3080-3082.
35. J. Arnold, Prog. Inorg. Chem., 1995, 43, 353-417.
36. O. L. Sydora, P. T. Wolczanski and E. B. Lobkovsky, Angew. Chem., Int. Ed., 2003, 42, 2685-2687.
37. G. A. Kraus and B. Andersh, Tetrahedron Lett., 1991, 32, 2189-2192.
38. M. Niemeyer and P. P. Power, Inorg. Chem., 1996, 35, 7264-7272.
39. (a) D. H. Grant, J. Chem. Educ., 1995, 72, 39-40;
40. (b) E. M. Schubert, J. Chem. Educ., 1992, 69, 62-63;
41. (c) D. F. Evans, J. Chem. Soc., 1959, 2003-2005.
42. G. J. P. Britovsek, V. C. Gibson, S. K. Spitzmesser, K. P. Tellmann, A. J. P. White and D. J. Williams, J. Chem. Soc., Dalton Trans., 2002, 1159-1171.
43. T. Komuro, T. Matsuo, H. Kawaguchi and K. Tatsumi, Inorg. Chem., 2003, 42, 5340-5347.
44. H. K. Lee, C. H. Lam, S.-L. Li, Z.-Y. Zhang and T. C. W. Mak, Inorg. Chem., 2001, 40, 4691-4695.
45. (a) D. T. Corwin, Jr., E. S. Gruff and S. A. Koch, J. Chem. Soc., Chem. Commun., 1987, 966-967;
46. (b) D. T. Corwin, Jr., R. Fikar and S. A. Koch, Inorg. Chem., 1987, 26, 3079-3080;
47. (c) G. Wei, M. Hong, Z. Huang and H. Liu, J. Chem. Soc., Dalton Trans., 1991, 3145-3148.
48. (a) E. Block, H. Rang, G. Ofori-Okai and J. Zubieta, Inorg. Chim. Acta, 1990, 167, 147-148;
49. (b) P. Espinet, M. C. Lequerica and J. M. Martin-Alvarez, Chem. Eur. J., 1999, 5, 1982-1986;
50. (c) J. Schneider, M. Köcherling, R. Kopitzky and G. Henkel, Eur. J. Inorg. Chem., 2003, 1727-1737;
51. (d) I. G. Dance, L. J. Fitzpatrick, D. C. Craig and M. L. Scudder, Inorg. Chem., 1989, 28, 1853-1861.
52. K. Tang, M. Aslam, E. Block, T. Nicholson and J. Zubieta, Inorg. Chem., 1987, 26, 1488-1497.
53. E. Block, M. Gernon, H. Kang, G. Ofori-Okai and J. Zubieta, Inorg. Chem., 1989, 28, 1263-1271.
54. E. G. Muller, S. F. Watkins and L. F. Dahl, J. Organomet. Chem., 1976, 111, 73-89.
55. R. M. Catala, M. E. Colsa, D. Cruzgarritz, H. Torrens, J. L. Brianso, J. E. Piniella and G. Germain, Transiton Met. Chem., 1987, 12, 197-199.
56. M. A. Usón and J. M. Llanos, J. Organomet. Chem., 2002, 663, 98-107.
57. (a) C. R. Lucas, M. J. Newlands, E. J. Gabe and F. L. Lee, Can. J. Chem., 1987, 65, 898-902;
58. (b) C. R. Lucas, Can. J. Chem., 1986, 64, 1758-1763;
59. (c) C. R. Lucas, Can. J. Chem., 1983, 61, 1096-1099;
60. (d) T. Matsuo and A. Sekiguchi, Bull. Chem. Soc. Jpn., 2004, 77, 211-226.
61. G. S. White and D. W. Stephan, Organometallics, 1988, 7, 903-910.
62. T. A. Wark and D. W. Stephan, Organometallics, 1989, 8, 2836-2843.
63. H. Sugiyama, Y. Hayashi, H. Kawaguchi and K. Tatsumi, Inorg. Chem., 1998, 37, 6773-6779.
64. (a) Crystal Structure Analysis Package, Rigaku and MSC, 2001;
65. (b) D. J. Watkin, C. K. Prout, J. R. Carruthers and P. W. Betteridge, Chemical Crystallography Laboratory, Oxford, UK.
66. H. D. Flack, Acta Crystallogr., Sect. A, 1983, 39, 876-881.