Synthesis group 10 polyfluorothiolate mono- and bi-nuclear complexes. Crystal structures of [Ni(SC 6 HF 4 ) 2 and[(dppe)Ni(μ-SC 6 F 5 ) 2 Pd (C 6 F 5 ) 2 ]

Journal of Organometallic Chemistry

Volumn 663, Issue 1-2, 2002, Pages 98-107

  Usón, Miguel A ^a   Llanos, Jesús M ^a  

^a UNIVERSITY OF ZARAGOZA   (Spain)

Author keywords

Crystal structures; Group 10; Homo and heterobinuclear; Organometallic compounds; Thiolates; interactions

Indexed keywords

ETHANE; FLUORENE DERIVATIVE; METHANE; PHOSPHINE DERIVATIVE; THIOL DERIVATIVE;

CHEMICAL ANALYSIS; CHEMICAL INTERACTION; CHEMICAL REACTION; COMPLEX FORMATION; CONTROLLED STUDY; CRYSTAL STRUCTURE; INFRARED SPECTROMETRY; ISOMER; MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; QUANTITATIVE ANALYSIS; REVIEW; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 0037011747     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(02)01734-5     Document Type: Article

References (29)

1. R. Usón, J. Forniés, L.R. Falvello, M.A. Usón, I. Usón, S. Herrero, Inorg. Chem. 32 (1993) 1066.
2. R. Usón, J. Forniés, M.A. Usón, M. Tomš, M.A. Ibanñez, J. Chem. Soc. Dalton Trans. (1994) 401.
3. R. Usón, J. Forniés, J. Fernández Sanz, M.A. Usón, I. Usón, S. Herrero, Inorg. Chem. 36 (1997) 1912.
4. S. Herrero, Ph.D. thesis, University of Zaragoza, 1996.
5. C.A. Hunter, J.K.M. Sanders, J. Am. Chem. Soc. 112 (1990) 5525.
6. R. Usón, J. Forniés, M.A. Usón, M.L. Mas, Inorg. Chim. Acta 168 (1990) 59 (and references cited therein).
7. R. Usón, J. Forniés, M.A. Usón, S. Herrero, J. Organomet. Chem. 447 (1993) 137.
8. J.A. Riddick, W.B. Bunger, Organic Solvents: Physical Properties and Methods of Purification, 3rd ed., Wiley-Interscience, New York, 1970.
9. M.E. Peach, Can. J. Chem. 46 (1968) 2699.
10. G.R. van Hecke, W.D. Horrocks, Jr., Inorg. Chem. 5 (1966) 1968.
11. A.R. Sanger, J. Chem. Soc. Dalton Trans. (1977) 1971.
12. T.G. Appleton, M.A. Bennet, I.B. Tomkin, J. Chem. Soc. Dalton Trans. (1976) 439.
13. R. Usón, J. Forniés, M. Tomás, B. Menjón, Organometallics 4 (1985) 1912.
14. M.A. Usón, J. Chem. Educ. 66 (1990) 412.
15. G.M. Sheldrick, SHELXTL PLUS, release 5.05, for Digital Alpha/VMS, Siemens Analytical X-Ray Instruments, Madison, WI, 1996.
16. G.M. Sheldrick, SHELXL-97: A Program for Crystal Structure Refinement, Universität Göttingen, BRD, 1997.
17. G.B. Deacon, J.H.S. Green, Spectrochim. Acta Part A 24 (1968) 1125.
18. D.A. Long, D. Steele, Spectrochim. Acta 19 (1963) 1955.
19. W. Beck, K.H. Stetter, S. Tadros, K.E. Schwarzhans, Chem. Ber. 100 (1967) 3944.
20. R. Moreno-Esparza, H. Torrens, M. Arroyo, J.L. Briansó, C. Miravitlles, J. Rius, Polyhedron 14 (1995) 1601.
21. J. Forniés, R. Navarro, E.P. Urriolabeitia, J. Organomet. Chem. 390 (1990) 257.
22. R. Usón, J. Forniés, M.A. Usón, J.A. Apaolaza, Inorg. Chim. Acta 187 (1991) 175.
23. R.M. Catalá, M.E. Colsa, D. Cruz-Garritz, H. Torrens, J.L. Brianso, J.E. Piniella, G. Germain, Transition Met. Chem. 12 (1987) 197 (refcode NACLUY).
24. Cambridge Structural Database, Cambridge Crystallographic Data Centre, University Chemical Laboratory, Cambridge, October 2001 Release for VMS.
25. R.O. Gould, P. Taylor, M.C. Thorpe, PUCKER, University of Edinburgh, UK, 1995.
26. R. Usön, J. Forniés, F. Martínez, M. Tomás, J. Chem. Soc. Dalton Trans. (1980) 888.
27. P.J. Blower, J.R. Dilworth, Coord. Chem. Rev. 76 (1987) 121.
28. E.W. Abel, S.K. Bhargava, K.G. Orrell, Prog. Inorg. Chem. 32 (1984) 1.
29. G. Sánchez, F. Momblona, M. Sánchez, J. Pérez, G. López, J. Casabó , E. Molins, C. Miravitlles, Eur. J. Inorg. Chem. (1998) 1199; refcode PUHKEI, retrieved from [24].