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Paganelli G., Zoboli S., Cremonesi M., Bodei L., Ferrari M., Grana C., Bartolomei M., Orsi F., De Cicco C., Macke H.R., Chinol M., de Braud F. Eur. J. Nucl. Med. 28:2001;426-434
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4
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2942679623
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note
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3-octreotide; Fmoc: 9-fluorenylmethyloxycarbonyl; HATU: O-(7-azabenzotriazol-1-yl)-N, N, N′, N′-tetramethyluronium hexafluorophosphate; HBTU: O-(1H-benzotriazol-1-yl)-N, N, N′, N′-tetramethyluronium hexafluorophosphate; ivDde: 1-(4, 4-dimethyl-2, 6-dioxocyclohex-1-ylidene)-3-methylbutyl; TIS: triisoproylsilane; TFA: trifluoroacetic acid
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5
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0033033382
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Heppeler A., Froidevaux S., Maecke H.R., Jermann E., Béhé M., Powell P., Hennig M. Chem. Eur. J. 5:1999;1974-1981
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Heppeler, A.1
Froidevaux, S.2
Maecke, H.R.3
Jermann, E.4
Béhé, M.5
Powell, P.6
Hennig, M.7
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9
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0037100020
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Graham K.A.N., Wang Q., Eisenhut M., Haberkorn U., Mier W. Tetrahedron Lett. 43:2002;5021-5024
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Graham, K.A.N.1
Wang, Q.2
Eisenhut, M.3
Haberkorn, U.4
Mier, W.5
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10
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1642574311
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Wang Q., Graham K., Schauer T., Fietz T., Mohammed A., Liu X., Hoffend J., Haberkorn U., Eisenhut M., Mier W. Nucl. Med. Biol. 31:2004;21-30
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Wang, Q.1
Graham, K.2
Schauer, T.3
Fietz, T.4
Mohammed, A.5
Liu, X.6
Hoffend, J.7
Haberkorn, U.8
Eisenhut, M.9
Mier, W.10
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11
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0037877997
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Mier W., Eritja R., Mohammed A., Haberkorn U., Eisenhut M. Angew. Chem., Int. Ed. 42:2003;1968-1971
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Mier, W.1
Eritja, R.2
Mohammed, A.3
Haberkorn, U.4
Eisenhut, M.5
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12
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2942648843
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Purchased from Novabiochem, Germany
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Purchased from Novabiochem, Germany
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13
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0032546258
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Chhabra S.R., Hothi B., Evans D.J., White P.D., Bycroft B.W., Chan W.C. Tetrahedron Lett. 39:1998;1603-1606
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Chhabra, S.R.1
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Evans, D.J.3
White, P.D.4
Bycroft, B.W.5
Chan, W.C.6
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Bycroft B.W., Chan W.C., Chhabra S.R., Hone N.D. J. Chem. Soc., Chem. Commun. 1993;778-779
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Bycroft, B.W.1
Chan, W.C.2
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Hone, N.D.4
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15
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2942690111
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Purchased from Macrocyclics, USA
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Purchased from Macrocyclics, USA
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16
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2942675203
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note
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4 pH 6.5, measuring the absorbancy at 280 nm
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17
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2942668578
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After lyophilisation 1-3 were obtained as white solids with overall yields of approximately 35%
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18
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2942642620
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note
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Molecular weight determinations were carried out on a matrix assisted laser desorption ionisation time-of-flight mass spectrometry (MALDI-3, Kratos Instruments) and electrospray mass spectrometry on a Finnigan MAT TSQ 7000
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19
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2942648844
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note
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3 was added. The solution was heated at 95°C for 25 min. A quality control of the radiolabelled peptides performed by HPLC showed yields >95% and a relative distribution of the label in accordance with the relative number of chelator moieties of the different species
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