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66
-
-
27844505385
-
-
note
-
-3. Remark: largest diff. peak near Br(6)(1.27 Å).
-
-
-
-
68
-
-
27844481768
-
-
note
-
+: 594.4094; found: 594.4092.
-
-
-
-
70
-
-
84859344280
-
-
(a) Martinez, A. G.; Barcina, J. O.; de Fresno Cerezo, A.; Subramanian, L. R. Synlett 1994, 1047.
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Martinez, A.G.1
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71
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0000350624
-
-
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Fouquet, E.1
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72
-
-
1842565056
-
-
(c) Mee, S. P. H.; Lee, V.; Baldwin, J. E. Angew. Chem. Int. Ed. 2004, 43, 1132.
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-
-
Mee, S.P.H.1
Lee, V.2
Baldwin, J.E.3
-
75
-
-
27844457305
-
-
note
-
4, concentrated, and purified by column chromatography.
-
-
-
-
76
-
-
27844588674
-
-
note
-
+: 493.2890; found: ! 493.2899.
-
-
-
-
77
-
-
27844474411
-
-
note
-
+: 750.2850; found: 750.2840.
-
-
-
-
78
-
-
27844534539
-
-
note
-
+]: 828.1141; found: 828.1133.
-
-
-
-
79
-
-
27844513579
-
-
note
-
+: 762.5033; found: 762.5022.
-
-
-
-
80
-
-
27844611622
-
-
note
-
+: 953.3109; found: 953.3116.
-
-
-
-
81
-
-
27844606149
-
-
note
-
3): δ = 28.58 (p), 59.01 (q), 89.38 (q), 124.32 (t), 125.90 (t), 126.22 (t), 126.86 (t), 127.20 (t), 133.47 (q), 133.69 (q), 142.94 (q), 143.07 (q), 146.28 (q), 151.17 (q). Various attempts to characterize 13 by mass spectrometry, including DEI, APCI and MALDI as ionization techniques, were unsuccessful.
-
-
-
-
82
-
-
0001248271
-
-
Kuck, D.; Schuster, A.; Krause, R. A. J. Org. Chem. 1991, 56, 3472.
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Kuck, D.1
Schuster, A.2
Krause, R.A.3
|