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2+H] calcd 619.14).
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4+H] calcd 721.18).
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4+H] calcd 719.17).
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38
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0141452964
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Crystals of Ni-3a were grown from dioxane-water at RT. Data were collected at 150(2) K with ω and öscans to approximately 56° 20 using an APEX II-FR591 diffractometer employing graphite-monochromated Mo-Kα radiation generated from a rotating anode (0.71073 Å). Data integration and reduction were undertaken with SAINT and XPREP [Bruker-Nonius (2003); APEX, SAINT and XPREP. Area detector control and data integration and reduction software. Bruker-Nonius Analytical X-ray Instruments Inc., Madison, WI, USA] and subsequent computations were carried out using the WinGX-32 [Farrugia, L. J. J. Appl. Crystallogr. 1999, 32, 837] graphical user interface. Scaling and a multi-scan empirical absorption correction were applied to the data using the program SADABS.
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