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note
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2 (0.239 g, 0.347 mmol) in 3 mL of diethyl ether was added dropwise to 0.5 wt % Na/Hg (2.3 equiv, 0.0182 g, 0.786 mmol) at -40°C. The mixture was stirred for 3 h at room temperature. The solvents were removed in vacuo, and the resulting solid was extracted with pentane. The mixture was filtered through Celite, and the solvents were removed from the filtrate in vacuo for a crude yield of 170 mg (81%). The sample can then be recrystallized from concentrated pentane containing a few drops of ether.
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Buda, C.4
Cundari, T.R.5
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23
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2442547607
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Tsang, W.C.P.1
Jamieson, J.Y.2
Aeilts, S.A.3
Hultzsch, K.C.4
Schrock, R.R.5
Hoveyda, A.H.6
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