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Volumn 24, Issue 22, 2005, Pages 5211-5213

Olefin metathesis reactions initiated by d 2 molybdenum or tungsten complexes

Author keywords

[No Author keywords available]

Indexed keywords

DIMERIC SPECIES; ETHYL GROUP; IMIDO COMPLEXES; METATHESIS;

EID: 27544439033     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om050583r     Document Type: Article
Times cited : (33)

References (23)
  • 13
    • 4143118459 scopus 로고    scopus 로고
    • Grubbs, R. H., Ed.; Wiley-VCH: Weinheim, Germany
    • Schrock, R. R. In Handbook of Metathesis; Grubbs, R. H., Ed.; Wiley-VCH: Weinheim, Germany, 2003; Vol. 1, p 173.
    • (2003) Handbook of Metathesis , vol.1 , pp. 173
    • Schrock, R.R.1
  • 14
    • 84861257001 scopus 로고    scopus 로고
    • Sinha, A.; Hock, A.; Müller, P. Unpublished results
    • Sinha, A.; Hock, A.; Müller, P. Unpublished results.
  • 15
    • 27544485076 scopus 로고    scopus 로고
    • Lopez, L. P. H. Unpublished results
    • Lopez, L. P. H. Unpublished results.
  • 20
    • 27544486420 scopus 로고    scopus 로고
    • note
    • 2 (0.239 g, 0.347 mmol) in 3 mL of diethyl ether was added dropwise to 0.5 wt % Na/Hg (2.3 equiv, 0.0182 g, 0.786 mmol) at -40°C. The mixture was stirred for 3 h at room temperature. The solvents were removed in vacuo, and the resulting solid was extracted with pentane. The mixture was filtered through Celite, and the solvents were removed from the filtrate in vacuo for a crude yield of 170 mg (81%). The sample can then be recrystallized from concentrated pentane containing a few drops of ether.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.