A solvent stabilized cyclic dimer complex of platinum(II) with S 2O2 macrocycle

Inorganic Chemistry Communications

Volumn 8, Issue 10, 2005, Pages 916-919

  Seo, Joobeom ^a   Yoon, Il ^a   Lee, Ji Eun ^a   Mi, Ryoung Song ^a   So, Young Lee ^a   Sun, Hong Park ^a   Tae, Ho Kim ^a   Park, Ki Min ^a   Bong, Gon Kim ^a   Lee, Shim Sung ^a  

^a Gyeongsang National University   (South Korea)

Author keywords

Crystal structure; Cyclic dimer complex; Entrapped dichloromethane; Hydrogen bond; Platinum(II); S2O2 macrocycle

Indexed keywords

EID: 24944581685     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2005.07.006     Document Type: Article

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28. 2 (0.050 g, 0.176 mmol) in dichloromethane (4 mL) were refluxed for 1 hour. The yellow precipitate formed was separated from the reaction mixture. The solid product was dissolved in acetonitrile and yellow crystals of 1 were obtained by slow evaporation of the solution in 50% yield. m.p. 269-270°C (decomp.).
29. 2+.
30. eq of the carrier atom.