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29
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2442596390
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note
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In case of phenylacetaldehyde increased yields in the AAD reaction were observed when toluene was used as solvent.
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30
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85088339077
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note
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2O was added to the reaction mixture to yield 1f.
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32
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2442545790
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note
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When 2d was employed, we obtained the isomer 4d as main product. Increasing the reaction time to 60 hours the desired 3d was obtained.
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