Determination of methyl and ethyl esters of methanesulfonic, benzenesulfonic and p-toluenesulfonic acids in active pharmaceutical ingredients by solid-phase microextraction (SPME) coupled to GC/SIM-MS

Journal of Pharmaceutical and Biomedical Analysis

Volumn 39, Issue 3-4, 2005, Pages 477-485

  Colón, Ivelisse ^a   Richoll, Stephen M ^a  

^a PFIZER INC   (United States)

Author keywords

Active pharmaceutical ingredients; Impurity analysis; LPME; Solid phase microextraction; SPE; SPME; Sulfonate esters; Sulfonic acid esters

Indexed keywords

BENZENESULFONIC ACID DERIVATIVE; ESTER; MESYLIC ACID ETHYL ESTER; MESYLIC ACID METHYL ESTER; SULFONIC ACID DERIVATIVE;

ACCURACY; ARTICLE; DRUG DETERMINATION; EXTRACTION; GAS CHROMATOGRAPHY; LIQUID LIQUID EXTRACTION; LIQUID PHASE MICROEXTRACTION; MASS SPECTROMETRY; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; REPRODUCIBILITY; SOLID PHASE MICROEXTRACTION; VALIDATION PROCESS;

BENZENESULFONATES; CHEMISTRY, PHARMACEUTICAL; CHROMATOGRAPHY; CHROMATOGRAPHY, GAS; DRUG INDUSTRY; ESTERS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HYDROGEN-ION CONCENTRATION; MESYLATES; PHOSPHATES; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; TIME FACTORS;

EID: 23944465208     PISSN: 07317085     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jpba.2005.04.037     Document Type: Article

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