Gas chromatography-high-resolution mass spectrometric method for determination of methamphetamine and its major metabolite amphetamine in human hair

Journal of Analytical Toxicology

Volumn 29, Issue 5, 2005, Pages 370-375

  Kim, Jin Young ^a,b   Suh, Sung Ill ^a   In, Moon Kyo ^a   Chung, Bong Chul ^c  

^a Forensic Science Division   (South Korea)

^b Yonsei University   (South Korea)

^c Korea Institute of Science and Technology   (South Korea)

Author keywords

[No Author keywords available]

Indexed keywords

AMPHETAMINE; METHAMPHETAMINE;

ACCURACY; CONFERENCE PAPER; CORRELATION COEFFICIENT; DRUG DETERMINATION; ESTHETIC SURGERY; GAS CHROMATOGRAPHY; HAIR; HAIR ANALYSIS; HUMAN; HUMAN TISSUE; ION MONITORING; MASS SPECTROMETRY; SENSITIVITY ANALYSIS; WASTE MANAGEMENT;

EID: 23944457933     PISSN: 01464760     EISSN: None     Source Type: Journal    
DOI: 10.1093/jat/29.5.370     Document Type: Conference Paper

References (41)

1. R.A. Glennon. Arylalkylamine drugs of abuse: an overview of drug discrimination studies. Pharmacol. Biochem. Behav. 64: 251-256 (1999).
2. B.I. Cho. Trends and patterns of methamphetamine abuse in the Republic of Korea. In NIDA Research Monographs 115 M.A. Miller and N.J. Kozel, Ed. Rockville, MD, 1991, pp 99-106.
3. Supreme Prosecutors' Office. White Paper on Drug-Related Crimes. Seoul, Korea, 2004, pp 95-104.
4. T. Mieczkowski, D. Barzelay, B. Gropper, and E. Wish. Concordance of three measures of cocaine use in an arrestee population: hair, urine, and self-report. J. Psychoactive Drugs 23: 241-249 (1991).
5. W.A. Baumgartner and V.A. Hill. Sample preparation techniques. Forensic Sci. Int. 63: 121-135 (1993)
6. Y. Gaillard, F. Vayssette, and G. Pépin. Compared interest between hair analysis and urinalysis in doping controls. Results for amphetamines, corticosteroids and anabolic steroids in racing cyclists. Forensic Sci. Int. 107: 361-379 (2000).
7. L. Skender. Hair-a biological source in drug analysis. Arh. Hig. Rada. Toksikol. 51: 409-420 (2000).
8. T. Nagai, M. Sato, T. Nagai, S. Kamiyama, and Y. Miura. A new analytical method for stereoisomers of methamphetamine and amphetamine and its application to forensic toxicology. Clin. Biochem. 22: 439-442 (1989).
9. N. Takayama, S. Tanaka, and K. Hayakawa. Determination of stimulants in a single human hair sample by high-performance liquid chromatographic method with chemiluminescence detection. Biomed. Chromatogr. 11: 25-28 (1997).
10. N. Takayama, S. Tanaka, R. Kizu, and K. Hayakawa. High-performance liquid chromatography study on effects of permanent wave, dye and decolorant treatments on methamphetamine and amphetamine in hair. Biomed. Chromatogr. 13: 257-261 (1999).
11. K. Nakashima, A. Kaddoumi, Y. Ishida, T. Itoh, and K. Taki. Determination of methamphetamine and amphetamine in abusers' plasma and hair samples with HPLC-FL. Biomed. Chromatogr. 17: 471-476 (2003).
12. A. Kaddoumi, R. Kikura-Hanajiri, and K. Nakashima. High-performance liquid chromatography with fluorescence detection for the simultaneous determination of 3,4-methylenedioxymethamphetamine, methamphetamine and their metabolites in human hair using DIB-Cl as a label. Biomed. Chromatogr. 18: 202-204 (2004).
13. I. Koide, O. Noguchi, K. Okada, A. Yokoyama, H. Oda, S. Yamamoto, and H. Kataoka. Determination of amphetamine and methamphetamine in human hair by headspace solid-phase microextraction and gas chromatography with nitrogen-phosphorus detection. J. Chromatogr. B 707: 99-104 (1998).
14. O. Suzuki, H. Hattori, and M. Asano. Detection of methamphetamine and amphetamine in a single human hair by gas chromatography/chemical ionization mass spectrometry. J. Forensic Sci. 29: 611-617 (1984).
15. Y. Nakahara, K. Takahashi, Y. Takeda, K. Konuma, S. Fukui, and T. Tokui. Hair analysis for drug abuse, Part II. Hair analysis for monitoring of methamphetamine abuse by isotope dilution gas chromatography/mass spectrometry. Forensic Sci. Int. 46: 243-254 (1990).
16. Y. Nakahara. Detection and diagnostic interpretation of amphetamines in hair. Forensic Sci. Int. 70: 135-153 (1995).
17. Y. Nakahara, K. Takahashi, and R. Kikura. Hair analysis for drugs of abuse. X. Effect of physicochemical properties of drugs on the incorporation rates into hair. Biol. Pharm. Bull. 18: 1223-1227 (1995).
18. P. Kintz and V. Cirimele. Related Interlaboratory comparison of quantitative determination of amphetamine and related compounds in hair samples. Forensic Sci. Int. 84: 151-156 (1997).
19. M. Rothe, F. Pragst, K. Spiegel, T. Harrach, K. Fischer, and J. Kunkel. Hair concentrations and self-reported abuse history of 20 amphetamine and ecstasy users. Forensic Sci. Int. 89: 111-128 (1997).
20. L. Skender, V. Karacic, I. Brcic, and A. Bagaric. Quantitative determination of amphetamines, cocaine, and opiates in human hair by gas chromatography/mass spectrometry. Forensic Sci. Int. 125: 120-126 (2002).
21. M. Nishida, A. Namera, M. Yashiki, and T. Kojima. Routine analysis of amphetamine and methamphetamine in biological materials by gas chromatography-mass spectrometry and on-column derivatization. J. Chromatogr. B 789: 65-71 (2003).
22. M.J. Welch, L.T. Sniegoski, and S. Tai. Two new standard reference materials for the determination of drugs of abuse in human hair. Anal. Bioanal. Chem. 376: 1205-1211 (2003).
23. M. Pujadas, S. Pichini, S. Poudevida, E. Menoyo, P. Zuccaro, M. Farre, and R. de la Torre. Development and validation of a gas chromatography-mass spectrometry assay for hair analysis of amphetamine, methamphetamine and methylenedioxy derivatives. J. Chromatogr. B 798: 249-255 (2003).
24. S. Gentili, M. Cornetta, and T. Macchia. Rapid screening procedure based on headspace solid-phase microextraction and gas chromatography-mass spectrometry for the detection of many recreational drugs in hair. J. Chromatogr. B 801: 289-296 (2004).
25. D. Scarcella, F. Tagliaro, S. Turrina, G. Manetto, Y. Nakahara, F.P. Smith, and M. Marigo. Optimization of a simple method for the chiral separation of phenethylamines of forensic interest based on cyclodextrin complexation capillary electrophoresis and its preliminary application to the analysis of human urine and hair. Forensic Sci. Int. 89: 33-46 (1997).
26. F. Tagliaro, G. Manetto, S. Bellini, D. Scarcella, P.P. Smith, and M. Marigo. Simultaneous chiral separation of 3,4-methylene-dioxymethamphetamine, 3-4-methylenedioxyamphetamine, 3,4-methylenedioxyethylamphetamine, ephedrine, amphetamine and methamphetamine by capillary electrophoresis in uncoated and coated capillaries with native beta-cyclodextrin as the chiral selector: preliminary application to the analysis of urine and hair. Electrophoresis 19: 42-50 (1998).
27. A. Miki, M. Katagi, and H. Tsuchihashi. Determination of methamphetamine and its metabolites incorporated in hair by column-switching liquid chromatography-mass spectrometry. J. Anal. Toxicol. 27: 95-102 (2003).
28. R. Stanaszek and W. Piekoszewski. Simultaneous determination of eight underivatized amphetamines in hair by high-performance liquid chromatography-atmospheric pressure chemical ionization mass spectrometry (HPLC-APCI-MS). J. Anal. Toxicol. 28: 77-85 (2004).
29. R. Kronstrand, I. Nyström, J. Strandberg, and H. Druid. Screening for drugs of abuse in hair with ion spray LC-MS-MS. Forensic Sci. Int. 145: 183-190 (2004).
30. L. Pötsch, G. Skopp, and J. Becker. Related ultrastructural alterations and environmental exposure influence the opiate concentrations in hair of drug addicts. Int. J. Legal Med. 107: 301-305 (1995).
31. V. Cirimele, P. Kintz, and P. Mangin. Drug concentrations in human hair after bleaching. J. Anal. Toxicol. 19: 331-332 (1995).
32. L. Pötsch and G. Skopp. Stability of opiates in hair fibers after exposure to cosmetic treatment. Forensic Sci. Int. 81: 95-102 (1996).
33. G. Skopp, L. Pötsch, and M.R. Moeller. On cosmetically treated hair-aspects and pitfalls of interpretation. Forensic Sci. Int. 84: 43-52 (1997).
34. C. Jurado, P. Kintz, M. Menéndez, and M. Repetto. Influence of the cosmetic treatment of hair on drug testing. Int. J. Legal Med. 110: 159-163 (1997).
35. N. Takayama, S. Tanaka, R. Kizu, and K. Hayakawa. High-performance liquid chromatography study on effects of permanent wave, dye and decolorant treatments on methamphetamine and amphetamine in hair. Biomed. Chromatogr. 13: 257-261 (1999).
36. M. Yegles, Y. Marson, and R. Wennig. Influence of bleaching on stability of benzodiazepines in hair. Forensic Sci. Int. 107: 87-92 (2000).
37. J.Y. Kim, M.K. In, K.-J. Paeng, and B.C. Chung. Simultaneous determination of nalbuphine and opiates in human hair by gas chromatography-mass spectrometry. Chromatographia 59: 219-226 (2004).
38. M.J. Welch, L.T. Sniegoski, C.C. Allgood, and M. Habram. Hair analysis for drugs of abuse: evaluation of analytical methods, environmental issues, and development of reference materials. J. Anal. Toxicol. 17: 389-398 (1993).
39. A. Polettini, A. Groppi, and M. Montagna. Rapid and highly selective GC/MS/MS detection of heroin and its metabolites in hair. Forensic Sci. Int. 63: 217-225 (1993).
40. M. Uhl. Tandem mass spectrometry: a helpful tool in hair analysis for the forensic expert. Forensic Sci. Int. 107: 169-179 (2000).
41. C. Jouvel, P. Maciejewski, P. Garcia, Y. Bonnaire, S. Horning, and M.A. Popot. Detection of diazepam in horse hair samples by mass spectrometric methods. Analyst 125: 1765-1769 (2000).