Development and validation of a gas chromatography-mass spectrometry assay for hair analysis of amphetamine, methamphetamine and methylenedioxy derivatives

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 798, Issue 2, 2003, Pages 249-255

  Pujadas, Mitona ^a   Pichini, Simona ^b,c   Poudevida, Sandra ^a   Menoyo, Ester ^a   Zuccaro, Piergiorgio ^b   Farré, Magí ^a,c   De La Torre, Rafael ^a,d  

^a INST MUNIC D INVESTIGACIO MEDICA   (Spain)

^b ISTITUTO SUPERIORE DI SANITÀ   (Italy)

^c UNIVERSITAT AUTÒNOMA DE BARCELONA   (Spain)

^d UNIVERSITAT POMPEU FABRA   (Spain)

Author keywords

Amphetamine; Derivatization, GC; Methamphetamine

Indexed keywords

AMINES; BIOASSAY; DERIVATIVES; EXTRACTION; MASS SPECTROMETRY; SODIUM COMPOUNDS; SPECTROMETERS;

INTRA-ASSAY ERRORS; SOLID PHASE EXTRACTION (SPE);

GAS CHROMATOGRAPHY;

3,4 METHYLENEDIOXYAMPHETAMINE; 3,4 METHYLENEDIOXYMETHAMPHETAMINE; AMPHETAMINE DERIVATIVE; METHAMPHETAMINE; SODIUM SULFIDE;

ADULT; ANALYTIC METHOD; ARTICLE; CLINICAL ARTICLE; CONTROLLED STUDY; DRUG ABUSE PATTERN; DRUG HAIR LEVEL; EXTRACTION; FUNCTIONAL ASSESSMENT; GAS LIQUID CHROMATOGRAPHY; HAIR ANALYSIS; HUMAN; HUMAN TISSUE; ION MONITORING; MASS FRAGMENTOGRAPHY; PRIORITY JOURNAL; PROTEIN DEGRADATION; REPRODUCIBILITY; ROOM TEMPERATURE; SOLID PHASE EXTRACTION;

EID: 0344845343     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2003.09.056     Document Type: Article

References (23)

1. Wright J.D., Pearl L. BMJ. 310:1995;20.
2. Zhao H., Brenneisen R., Scholer A., McNally A., Elsohly M.A., Murphy T., Salamone S.J. J. Anal. Toxicol. 25:2001;258.
3. McCann U., Slate S.O., Ricaurte G.A. Drug Saf. 15:1996;107.
4. Henry J.A., Jeffreys K.J., Dawling S. Lancet. 340:1992;384.
5. Kraemer T., Maurer H.H. J. Chromatogr. Biomed. Appl. 713:1998;163.
6. Pichini S., Altieri I., Zuccaro P., Pacifici R. Clin. Pharmacokinet. 30:1996;211.
7. McHenna D.J., Peroutka S.J. J. Neurochem. 54:1990;14.
8. Kintz P., Cirimele V., Tracqui A., Mangin P. J. Chromatogr. Biomed. Appl. 670:1995;162.
9. Nakahara Y. Forensic Sci. Int. 70:1995;135.
10. Rothe M., Pragst F., Spiegel K., Harrach T., Fischer K., Kunkel J. Forensic Sci. Int. 89:1997;111.
11. Kronstrand R., Grundin R., Jonsson J. Forensic Sci. Int. 92:1998;29.
12. Cooper G.A.A., Allen D.L., Scott K.S., Oliver J.S., Ditton J., Smith I.D. J. Forensic Sci. 45:2000;400.
13. Sachs H., Kintz P. J. Chromatogr. B. 713:1998;147.
14. Röhrich J., Kauert G. Forensic Sci. Int. 84:1997;179.
15. Kintz P., Samyn N. J. Chromatogr. B. 733:1999;137.
16. Liu J., Hara K., Kashimura S., Kashiwagi M., Kageura M. J. Chromatogr. B. 758:2001;95.
17. Guidance for Industry, Bioanalytical Method Validation, US Department of Health and Human Services, Food and Drug Administration, May 2001 ( http://www.fda.gov/cder/guidance/4252fnl.htm ).
18. Claffey D.J., Stout P.R., Ruth J.A. J. Anal. Toxicol. 24:2000;54.
19. Ortuño J., Pizarro N., Farré M., Mas M., Segura J., Camí J., Brenneisen R., de la Torre R. J. Chromatogr. B. 723:1999;221.
20. Kikura R., Nakahara Y. Biol. Pharm. Bull. 18:1995;1694.
21. Segura J., Stramesi C., Redón A., Ventura M., Sánchez C.J., González G., San L., Montagna M. J. Chromatogr. B. 724:1999;9.
22. Kintz P., Cirimele V. Forensic Sci. Int. 84:1997;151.
23. Kronstrand R., Förstberg-Peterson S., Kågedal B., Ahlner J., Larson G. Clin. Chem. 45:1999;1485.