The determination of 2β-(3-hydroxypropoxy)-1α,25-dihydroxy vitamin D3 (ED-71) in human serum by high-performance liquid chromatography-electrospray tandem mass spectrometry

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 823, Issue 2, 2005, Pages 61-68

  Murao, Naoaki ^a   Ohishi, Norihisa ^a   Nabuchi, Yoshiaki ^a   Ishigai, Masaki ^a   Kawanishi, Takehiko ^a   Aso, Yoshinori ^a  

^a CHUGAI PHARMACEUTICAL CO LTD   (Japan)

Author keywords

2 (3 Hydroxypropoxy) 1 ,25 dihydroxy vitamin D3 (ED 71); Human serum; LC ESI MS MS; preED 71

Indexed keywords

BODY FLUIDS; CALIBRATION; EXTRACTION; IONIZATION; MASS SPECTROMETRY; METHANOL; PHARMACOKINETICS; VITAMINS;

HUMAN SERUM; LC/ESI-MS/MS; PREED-71; SOLID-PHASE EXTRACTION;

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

2BETA (3 HYDROXYPROPOXY)CALCITRIOL; AMINE; AMMONIUM ACETATE; ION; METHANOL; 2 (3 HYDROXYPROPOXY) 1,25 DIHYDROXYVITAMIN D3; 2-(3-HYDROXYPROPOXY)-1,25-DIHYDROXYVITAMIN D3; CALCITRIOL; DRUG DERIVATIVE;

ACCURACY; ANALYTIC METHOD; ARTICLE; BIOLOGICAL ACTIVITY; BLOOD SAMPLING; CALIBRATION; COLUMN CHROMATOGRAPHY; CONTROLLED STUDY; ELECTROSPRAY MASS SPECTROMETRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; HUMAN EXPERIMENT; ISOMER; LINEAR SYSTEM; NORMAL HUMAN; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; REACTION ANALYSIS; REPRODUCIBILITY; SEPARATION TECHNIQUE; SERUM; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; VITAMIN BLOOD LEVEL; BLOOD; COMPARATIVE STUDY; METHODOLOGY; TEMPERATURE; TIME;

CALCITRIOL; CALIBRATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; HUMANS; REPRODUCIBILITY OF RESULTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TEMPERATURE; TIME FACTORS;

EID: 23644437309     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2004.10.066     Document Type: Article

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