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Volumn , Issue 6, 2004, Pages 967-969

Preparation of (2-methyl-propane-2-sulfonylimino) acetic acid ethyl ester

Author keywords

Allylation; Amino acids; Imino ester

Indexed keywords

ACETIC ACID; CHLORINE COMPOUNDS; SYNTHESIS (CHEMICAL);

EID: 2342607541     PISSN: 00397881     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-2004-815925     Document Type: Article
Times cited : (11)

References (48)
  • 7
    • 0032484179 scopus 로고    scopus 로고
    • (a) Yao, S.; Johannsen, M.; Hazell, R. G.; Jorgensen, K. A. Angew. Chem. Int. Ed. 1998, 37, 3121; Angew. Chem. 1998, 110, 3318.
    • (1998) Angew. Chem. , vol.110 , pp. 3318
  • 9
    • 0034675619 scopus 로고    scopus 로고
    • (b) Jørgensen, K. A. Angew. Chem., Int. Ed. 2000, 39, 3558; Angew. Chem. 2000, 112, 3702.
    • (2000) Angew. Chem. , vol.112 , pp. 3702
  • 20
    • 0035902842 scopus 로고    scopus 로고
    • (a) Juhl, K.; Gathergood, N.; Jørgensen, K. A. Angew. Chem., Int. Ed. 2001, 40, 2995; Angew. Chem. 2001, 113, 3083.
    • (2001) Angew. Chem. , vol.113 , pp. 3083
  • 25
    • 0034680630 scopus 로고    scopus 로고
    • (a) Saaby, S.; Fang, X.; Gathergood, N.; Jørgensen, K. A. Angew. Chem., Int. Ed. 2000, 39, 4114; Angew. Chem. 2000, 112, 4280.
    • (2000) Angew. Chem. , vol.112 , pp. 4280
  • 46
    • 2342604719 scopus 로고    scopus 로고
    • If desired 5 can be isolated, see ref. 13
    • If desired 5 can be isolated, see ref. 13
  • 48
    • 2342606779 scopus 로고    scopus 로고
    • note
    • A technical 50% solution of ethyl glyoxylate in toluene was concentrated at atmospheric pressure and the residue was distilled to give ethyl glyoxylate as a turbid yellow oil. A second distillation of this material at atmospheric pressure by using a 20 cm Vigreux column at a bath temperature of 160-180°C furnished ethyl glyoxylate as a yellow fluid, which was used immediately and transferred to the reaction mixture by a syringe.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.