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1H NMR were found to be higher at 192 and 329, respectively. This is undoubtedly due to the fact that our experiments are carried out in neat epoxide, where at the termination of the copolymerization process free epoxide is the dominant signal in the NMR spectrum.
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33044499108
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4NCl salt as cocatalyst, there was some copolymer isolated (polymer:cyclic ratio was 25:75).
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37
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33044490992
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note
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Bis(triphenylphosphoranylide)ammonium][N, N′-bis(3,5-di-tert-butyl- salicylidene)-1,2-ethylene-diiminechromium(III)bis-azide] has been isolated and crystallographically characterized in our laboratory by Ryan M. Mackiewicz.
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