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32744473005
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note
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(a) Presence of CO was checked with an electrochemical cell CO detector.
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23
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32744472892
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note
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2.
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32744473067
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note
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Nitroxide-substituted species (doublets) were calculated at the UHF level. ZPE correction was applied to all stationary points.
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29
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32744454469
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note
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All attempts to detect metal paramagnetic species by low-temperature EPR have been unsuccessful, and this can be attributed to the large excess of nitroxyl radical present in the reaction media and to the expected low concentration of doublet species such as I.
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