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39
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3743088672
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note
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At zirconocene concentrations above 1 mmol/L, a red oil precipitates shortly after.
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41
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note
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d ≈ 1.3 is expected.
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13C NMR spectra of the oligomers, a multitude of unassignable signals are apparent, presumably due to the presence of widely varying degrees of oligomerization and stereoregularity. Changes observed in the spectra of the deuterated products were thus not assignable either.
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