메뉴 건너뛰기




Volumn 46, Issue 27, 2005, Pages 4555-4558

Niobium(V) chloride catalyzed microwave assisted synthesis of 2,3-unsaturated O-glycosides by the Ferrier reaction

Author keywords

[No Author keywords available]

Indexed keywords

ALCOHOL DERIVATIVE; GLYCOSIDE; NIOBIUM;

EID: 20344392649     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2005.05.015     Document Type: Article
Times cited : (49)

References (45)
  • 41
    • 20344399266 scopus 로고    scopus 로고
    • note
    • 5 (0.01 mmol) and the mixture irradiated with microwaves (Kenstar Model No. OM-9918C; 2450 MHz, 2350 W) for the specified period of time in an open vessel. After completion of the reaction, the reaction mixture was diluted with water and extracted twice with ethyl acetate. The combined organic extracts were dried over anhydrous sodium sulphate and concentrated in vacuo. The product was purified by silica gel column chromatography using ethyl acetate and light petroleum (60-80°C)
  • 45
    • 20344367143 scopus 로고    scopus 로고
    • note
    • 13C NMR and CHNS analysis


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.