Thermolysis of the tetrahedrane cluster PhCCo3(CO) 3(μ-CO)Cp2 with the unsaturated diphosphine ligands (Z)-Ph2PCH=CHPPh2 and 4,5-Bis(diphenylphosphino)-4- cyclopenten-1,3-dione (bpcd): Redox properties and molecular structure of PhCCo3(CO)(μ-CO)[(Z)-Ph2PCH=CHPPh2]Cp 2

Journal of Chemical Crystallography

Volumn 35, Issue 2, 2005, Pages 157-165

  Watson, William H ^a,b   Kandala, Srikanth ^b   Richmond, Michael G ^a,b  

^a TEXAS CHRISTIAN UNIVERSITY   (United States)

^b UNIVERSITY OF NORTH TEXAS   (United States)

Author keywords

Cobalt cluster; Diphosphine ligands; Ligand substitution; Redox chemistry

Indexed keywords

LIGAND; PHOSPHINE DERIVATIVE;

ARTICLE; CHEMICAL BOND; CRYSTAL STRUCTURE; CYCLIC POTENTIOMETRY; ELECTRON; INFRARED SPECTROSCOPY; OXIDATION REDUCTION REACTION; PHOSPHORUS NUCLEAR MAGNETIC RESONANCE; PROTON NUCLEAR MAGNETIC RESONANCE; STRUCTURE ANALYSIS; X RAY CRYSTALLOGRAPHY;

EID: 17744370972     PISSN: 10741542     EISSN: None     Source Type: Journal    
DOI: 10.1007/s10870-005-2806-3     Document Type: Article

References (36)

1. Elder, P.A.; Robinson, B.H.; Simpson, J. J. Chem. Soc., Dalton Trans. 1975, 1771.
2. Sutin, K.A.; Faggiani, R.; McGlinchey, M.J. New J. Chem. 1988, 12, 419.
3. Yuan, P.; Richmond, M.G.; Schwartz, M. Inorg. Chem. 1991, 30, 679.
4. (a) Fenske, D.; Becher, H. Chem. Ber. 1974, 107, 117.
5. (b) Fenske, D. Chem. Ber. 1979, 112, 363.
6. Shriver, D.F. The Manipulation of Air-Sensitive Compounds; McGraw-Hill: New York, 1969.
7. Saint Version 6.02; Bruker Analytical X-ray Systems; Madison, WI, USA Copyright 1997-1999.
8. SHELXTL Version 5.1; Bruker Analytical X-ray Systems; Madison, WI, USA Copyright 1998.
9. Speck, A.L. PLATON - A Multipurpose Crystallographic Tool; Utrecht University: Utrecht, The Netherlands, 2001.
10. Ryan, M.F.; Richardson, D.E.; Lichtenberger, D.L.; Gruhn, N.E. Organometallics 1994, 13, 1190.
11. (a) Hoffmann, R.; Lipscomb, W.H. J. Chem. Phys. 1962, 36, 2179.
12. (b) Hoffmann, R. J. Chem. Phys. 1963, 39, 1397.
13. Mealli, C.; Proserpio, D.M. J. Chem. Educ. 1990, 67, 399.
14. Weast, R.C., Ed. Handbook of Chemistry and Physics, 56th, edn.; CRC: Cleveland, OH, 1975.
15. Bott, S.G.; Yang, K.; Richmond, M.G. Organometallics 2003, 22, 1383.
16. Rao, C.N.R. Chemical Applications of Infrared Spectroscopy; Academic: New York, 1963.
17. Shen, H.; Bott, S.G.; Richmond, M.G. Inorg. Chim. Acta 1996, 241, 71.
18. Bott, S.G.; Wang, J.C.; Shen, H.; Richmond, M.G. J. Chem. Crystallogr. 1999, 29, 391.
19. McCallum, R.S.; Penfold, P.R. Acta Crystallogr. 1978, B34, 1688.
20. (a) Yang, K.; Bott, S.G.; Richmond, M.G. Organometallics 1994, 13, 3788.
21. (b) Bott, S.G.; Yang, K.; Richmond, M.G. J. Chem. Crystallogr. 2000, 30, 627.
22. (c) Watson, W.H.; Ejsmont, K.; Liu, J.; Richmond, M.G. J. Chem. Crystallogr. 2003, 33, 775.
23. Horwitz, C.P.; Shriver, D.F. Adv. Organomet. Chem. 1984, 23, 219.
24. Orpen, A.G.; Bramer, L.; Allen, F.H.; Kennard, O.; Watson, D.G.; Taylor, R. J. Chem. Soc., Dalton Trans. 1989, S1.
25. Bard, A.J.; Faulkner, L.R. Electrochemical Methods; Wiley: New York, 1980.
26. (a) Christie, J.H. J. Electroanal. Chem. 1967, 13, 79.
27. (b) Ridgeway, T.H.; van Duyne, R.P.; Reilley, C.N. J. Electroanal. Chem. 1972, 34, 267.
28. Duffy, N.W.; Nelson, R.R.; Richmond, M.G.; Rieger, A.L.; Rieger, P.H.; Robinson, B.H.; Tyler, D.R.; Wang, J.C.; Yang, K. Inorg. Chem. 1998, 37, 4849.
29. (a) Schilling, B.E.R.; Hoffmann, R. J. Am. Chem. Soc. 1979, 101, 3456.
30. (b) Strouse, C.E.; Dahl, L.F. J. Am. Chem. Soc. 1971, 93, 6032.
31. (c) Peake, B.M.; Robinson, B.H.; Simpson, J.; Watson, D.J. Inorg. Chem. 1977, 16, 405.
32. (d) Peake, B.M.; Rieger, P.H.; Robinson, B.H.; Simpson, J. Inorg. Chem. 1979, 78, 1000.
33. (e) Beurich, H.; Madach, T.; Richter, F.; Vahrenkamp, H. Angew. Chem. 1979, 91, 751.
34. (a) Bond, A.M.; Dawson, P.A.; Peake, B.M.; Rieger, P.H.; Robinson, B.H.; Simpson, J. Inorg. Chem. 1979, 18, 1413.
35. (b) Richmond, M.G.; Kochi, J.K. Inorg. Chem. 1986, 25, 656.
36. Gimarc, B.M. Molecular Structure and Bonding; Academic: New York, 1979.