Radiation damage analysis of 7,7,8,8,-tetracyanoquinodimethane (TCNQ) and 2,3,5,6,-tetrafluoro-7,7,8,8,-tetracyanoquinodimethane (F4TCNQ) by electron diffraction and electron energy loss spectroscopy

Micron

Volumn 36, Issue 3, 2005, Pages 271-279

  Koshino, Masanori ^a   Masunaga, Yuko Hasegawa ^a   Nemoto, Takashi ^a   Kurata, Hiroki ^a   Isoda, Seiij ^a  

^a KYOTO UNIVERSITY   (Japan)

Author keywords

Carbon K edge EELS; DV X calculation; Fluorinated TCNQ; Molecular occupancy; Radiation damage

Indexed keywords

BONDING; CROSSLINKING; DOSIMETRY; ELECTRON DIFFRACTION; ELECTRON ENERGY LOSS SPECTROSCOPY; ELECTRON IRRADIATION; FLUORINE; HYDROGEN; RADIATION DAMAGE; SUBSTITUTION REACTIONS;

7,7,8,8.-TETRAACYANOQUINODIMETHANE (TCNQ); INTERMOLECULAR SPACE; MASS LOSSES; MOLECULAR OCCUPANCY;

AROMATIC COMPOUNDS;

ANGUILLIFORMES;

EID: 13944283748     PISSN: 09684328     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.micron.2004.12.007     Document Type: Article

References (31)

1. A. Bondi Van der Waals volumes and radii Journal of Physical Chemistry 68 1964 441 451
2. B.J. Ciliax, K.L. Kirk, and R.D. Leapman Radiation damage of fluorinated organic compounds measured by parallel electron energy loss spectroscopy Ultramicroscopy 48 1993 13 25
3. W.R.K. Clark, J.N. Chapman, A.M. Macleod, and R.P. Ferrier Radiation damage mechanisms in copper phthalocyanine and its chlorinated derivatives Ultramicroscopy 5 1980 195 208
4. H. Daniels, A. Brown, A. Scott, T. Nichells, B. Rand, and R. Brydson Experimental and theoretical evidence for the magic angle in transmission electron energy loss spectroscopy Ultramicroscopy 96 2003 523 534
5. R.F. Egerton Chemical measurements of radiation damage in organic samples at and below room temperature Ultramicroscopy 5 1980 521 523
6. R.F. Egerton Measurement of radiation damage by electron energy-loss spectroscopy Journal of Microscopy 118 1980 389 399
7. R.F. Egerton Organic mass loss at 100 K and 300 K Journal of Microscopy 126 1982 95 100
8. Egerton, R.F., 1996. Electron Energy-Loss Spectroscopy in the Electron Microscope, 2nd ed. Plenum Press, New York and London.
9. R.F. Egerton, and I. Rauf Dose-rate dependence of electron- induced mass loss from organic specimens Ultramicroscopy 80 1999 247 254
10. 4. Evidence for long-range amphoteric intermolecular interactions and low dimensionality in the solid state structure Molecular Crystal and Liquid Crystal 65 1981 161 178
11. J.R. Fryer Radiation damage in organic crystalline films Ultramicroscopy 14 1984 227 236
12. J.R. Fryer, C.H. McConnell, F. Zemlin, and D.L. Dorset Effect of temperature on radiation damage to aromatic organic molecules Ultramicroscopy 40 1992 163 169
13. R.M. Glaeser Radiation damage and biological electron microscopy B.M. Siegel D.R. Beaman Physical Aspects of Electron Microscopy and Microbeam Analysis 1975 Wiley New York 205 229
14. M.S. Isaacson Inelastic scattering and beam damage of biological molecules B.M. Siege D.R. Beaman Physical Aspects of Electron Microscopy and Microbeam Analysis 1975 Wiley New York 247 258
15. M.S. Isaacson Specimen damage in the electron microscope M.A. Hayat Principles and Techniques of Electron Microscopy, Biological Application 1977 Van Nostrand Reinhold New York 1 78
16. Isoda, S., Ichida, T., Kawaguchi, A., Katayama, K. 1983. Crystal Structure of Poly(2-chloro-p-xylylene). Bulletin of the Institute for Chemical Research, Kyoto University 61, 222-228.
17. B. Jouffrey, P. Schattschneider, and C. Hebert The magic angle: a solved mystery Ultramicroscopy 102 2004 61 66
18. T. Kobayashi, T. Ogawa, S. Moriguchi, T. Suga, K. Yoshida, H. Kurata, and S. Isoda Inhomogeneous substitution of polyhalogenated copper-phthalocyanine studied by high-resolution imaging and electron crystallography Journal of Electron Microscopy 52 2003 85 90
19. 4TCNQ) Journal of Electron Spectroscopy and Related Phenomena 135 2004 191 200
20. H. Kurata, S. Isoda, and T. Kobayashi Eels study of radiation damage in chlorinated Cu-phthalocyanine and poly GeO-phthalocyanine Ultramicroscopy 41 1992 33 40
21. R.E. Long, R.A. Sparks, and K.N. Trueblood The crystal and molecular structure of 7,7,8,8- tetracyanoquinodimethane Acta Crystallographica 18 1965 932 939
22. M. Misra, and R.F. Egerton Assessment of electron irradiation damage to biomolecules by electron diffraction and electron energy-loss spectroscopy Ultramicroscopy 15 1984 337 344
23. E. Orti, R. Viruela, and P.M. Viruela Influence of benzoannulation on the molecular and electronic structures of tetracyanoquinodimethanes Journal of Physical Chemistry 100 1996 6138 6146
24. L. Reimer Review of the radiation damage problem of organic specimens in electron microscopy B.M. Siegel D.R. Beaman Physical Aspects of Electron Microscopy and Microbeam Analysis 1975 Wiley New York 231 245
25. L. Reimer Transmission Electron Microscopy 1997 Springer New York
26. L. Reimer, and J. Spruth Information about the radiation damage of organic molecules by electron diffraction Journal de Microscopie et de Spectroscopie Electroniques 3 1978 579 590
27. L. Reimer, and J. Spruth Interpretation of the fading of diffraction patterns from organic substances irradiated with 100 KeV electrons at 10-300 K Ultramicroscopy 10 1982 199 210
28. D.J. Smith, J.R. Fryer, and R.A. Camps Radiation damage and structural studies: halogenated phthalocyanines Ultramicroscopy 19 1986 279 297
29. Uyeda, N., Kobayashi, T., Ohara, M., Watanabe, M., Taoka, T., Harada, Y., 1972. Effect of accelerating voltage and specimen temperature on radiation damage of hexadecachloro copper phthalocyanine. In, fifth European congress on electron microscopy, London, p. 566.
30. R.H. Wade, and J. Pelissier The temperature dependence of the electron irradiation resistance of crystalline paraffin Ultramicroscopy 10 1982 285 290
31. L. Zuppiroli, N. Housseau, L. Forro, J.P. Guillot, and J. Pelissier Fading of the Braggs spots in irradiated organic conductors: temperature and composition effects Ultramicroscopy 19 1986 325 336