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This MCC was based on some earlier studies performed by the group of Cacchi and Arcadi: Arcadi, A.; Cacchi, S.; Del Rosario, M.; Fabrizi, G.; Marinelli, F. J. Org. Chem. 1996, 61, 9280
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1342328275
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note
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int = 0.050), 1811 with I > 3σ(I) used in refinement. The final R = 0.029 and wR = 0.034 for the reflections used in the refinement. X-ray diffraction data were collected on a Nonius Kappa CCD diffractometer (graphite monochromator, λ = 0.71073 Å). Structure solution was by direct methods and refinement completed by full-matrix least-squares on F. Non-hydrogen atoms were refined with anisotropic displacement parameters, and hydrogen atoms were included at calculated positions and ride on the atoms to which they are bonded. The crystallographic data have been deposited with the Cambridge Crystallographic Data Center (CCDC 227359).
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21
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0001581454
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Westermann, J.2
Kyung, S.3
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22
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1342264428
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note
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2 to give III. Based on the results of this study, such a modification of the Reetz protocol may not be necessary.
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23
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0002636574
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A sample of a chiral N,P-chelated iridium catalyst was kindly supplied to us by this group. However, this catayst appeared to be inhibited by 18 since even known substrates were not able to be hydrogenated in the presence of a small amount of 18
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Menges, F.; Pfaltz, A. Adv. Synth. Catal. 2002, 344, 40. A sample of a chiral N,P-chelated iridium catalyst was kindly supplied to us by this group. However, this catayst appeared to be inhibited by 18 since even known substrates were not able to be hydrogenated in the presence of a small amount of 18.
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Adv. Synth. Catal.
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Menges, F.1
Pfaltz, A.2
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