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Volumn 46, Issue 6, 2005, Pages 979-982

A mild and efficient method for the synthesis of vinylogous carbamates from alkyl azides

Author keywords

Alkyl azide; Enaminone; Hydrogenation

Indexed keywords

AZIDE; CARBAMIC ACID DERIVATIVE; HETEROCYCLIC COMPOUND; HYDROGEN;

EID: 12344337360     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2004.12.047     Document Type: Article
Times cited : (29)

References (48)
  • 7
    • 0004087670 scopus 로고
    • John Wiley and Sons Chichester, New York, Brisbane, Toronto, Singapore
    • Z. Rappoport The Chemistry of Enamines Part 1 1994 John Wiley and Sons Chichester, New York, Brisbane, Toronto, Singapore
    • (1994) The Chemistry of Enamines Part 1
    • Rappoport, Z.1
  • 40
    • 85187114981 scopus 로고    scopus 로고
    • note
    • To a solution of alkyl azide (1 equiv) and methyl acetoacetate (2 equiv) in EtOAc was added a catalytic amount of 10% Pd/C (∼10% weight) and the reaction mixture was stirred under hydrogen (balloon) at room temperature. After 0.5-2 h, the catalyst was filtered off and the residue obtained after the removal of all volatiles, passed through a small silica gel plug to furnish the desired products as a Z:E mixture
  • 45
    • 85187105231 scopus 로고    scopus 로고
    • note
    • See supporting information for characterization of all new compounds characterization
  • 48
    • 85187113828 scopus 로고    scopus 로고
    • note
    • This reaction was not optimised


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.