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2,5-Dimethyl-α-chloroacetophenone was synthesized according to ref 13
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2,5-Dimethyl-α-chloroacetophenone was synthesized according to ref 13.
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27
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85037446630
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note
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10O: C, 82.16; H, 6.89. Found: C, 82.39; H, 6.92.
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28
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85037468279
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note
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2: C, 74.13; H, 7.92. Found: C, 73.91; H, 7.96.
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85037451950
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-
note
-
Samples in Pyrex tubes were degassed in three freeze - pump - thaw cycles before being sealed and were irradiated in a "merry-go-round" apparatus immersed in a water bath. The 366 nm band from a medium-pressure 125 W Teslamp mercury lamp was isolated by filtration with Corning CS 0-52 and CS 7-37 filters.
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34
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0033554022
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