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Volumn 42, Issue 6, 2003, Pages 643-647

A layered nickel succinate with unprecedented hexanickel units: Structure elucidation from powder-diffraction data, and magnetic and sorption properties

Author keywords

Carboxylate ligands; Hydrothermal synthesis; Magnetic properties; Microporous materials; Nickel; X ray powder diffraction

Indexed keywords

ATOMS; CRYSTAL ATOMIC STRUCTURE; IONS;

EID: 0037429426     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.200390177     Document Type: Article
Times cited : (49)

References (45)
  • 1
  • 16
    • 0035800381 scopus 로고    scopus 로고
    • b) N. Guillou, Q. Gao, P. M. Forster, J.-S Chang, M. Noguès, S.-E. Park, G. Férey, A. K. Cheetham, Angew. Chem. 2001, 113, 2913-2916; Angew. Chem. Int. Ed. 2001, 40, 2831-2834.
    • (2001) Angew. Chem. Int. Ed. , vol.40 , pp. 2831-2834
  • 18
    • 0036469851 scopus 로고    scopus 로고
    • P. M. Forster, A. K. Cheetham, Angew. Chem. 2002, 114, 475-477; Angew. Chem. Int. Ed. 2002, 41, 457-459.
    • (2002) Angew. Chem. Int. Ed. , vol.41 , pp. 457-459
  • 21
    • 0037012753 scopus 로고    scopus 로고
    • b) S. Konar P. S. Mukherjee, E. Zangrando, F. Lloret, N. R. Chaudhuri, Angew. Chem. 2002, 114, 1631-1633; Angew. Chem. Int. Ed. 2002, 41, 1561-1563;
    • (2002) Angew. Chem. Int. Ed. , vol.41 , pp. 1561-1563
  • 24
    • 85086812382 scopus 로고    scopus 로고
    • note
    • 2O (5 mL) in the molar ratio 1:1.5:4.1:120. After cooling (pH 6), the pale green powder was washed with distilled water. Elemental analysis (%): calcd: C 16.60, H 3.66, Ni 35.49; found: C 16.65, H 3.66, Ni 33.80.
  • 25
    • 0026368044 scopus 로고
    • High-resolution synchrotron data were measured with a Debye-Scherrer diffractometer geometry and a Si(111) analyzer crystal (λ = 0.7999 Å). The powder was introduced in a 1.5 mm capillary and the pattern was scanned in the range 2 θ = 1-60° with a step length of 2 θ = 0.0035° and a counting time of 1 s per step. To improve the counting statistics at high angles, the pattern was then divided in two 2 θ regions (1-15 and 15-45°), with times per step of 1 and 3 s, respectively. Pattern indexing was carried out with DICVOL91 (A. Boultif, D. Louër, J. Appl. Crystallogr. 1991, 24, 987-993). Direct methods and Fourier difference calculations were performed with SHELXTL (G. M. Sheldrick, 1997). Pattern matching and Rietveld refinements were performed by using FullProf (J. Rodriguez-Carvajal in Collected Abstract of Powder Diffraction Meeting (Toulouse), 1990, p. 127) and integrated in WinPlotr (T. Roisnel, J. Rodriguez-Carvajal, Mater. Sci. Forum 2001, 378-381, 118-123). CCDC-194049 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge vía www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Center, 12, Union Road, Cambridge CB21EZ, UK; fax: (+44)1223-336-033; or deposit@ccdc.cam.ac.uk).
    • (1991) J. Appl. Crystallogr. , vol.24 , pp. 987-993
    • Boultif, A.1    Louër, D.2
  • 26
    • 0026368044 scopus 로고
    • Toulouse
    • High-resolution synchrotron data were measured with a Debye-Scherrer diffractometer geometry and a Si(111) analyzer crystal (λ = 0.7999 Å). The powder was introduced in a 1.5 mm capillary and the pattern was scanned in the range 2 θ = 1-60° with a step length of 2 θ = 0.0035° and a counting time of 1 s per step. To improve the counting statistics at high angles, the pattern was then divided in two 2 θ regions (1-15 and 15-45°), with times per step of 1 and 3 s, respectively. Pattern indexing was carried out with DICVOL91 (A. Boultif, D. Louër, J. Appl. Crystallogr. 1991, 24, 987-993). Direct methods and Fourier difference calculations were performed with SHELXTL (G. M. Sheldrick, 1997). Pattern matching and Rietveld refinements were performed by using FullProf (J. Rodriguez-Carvajal in Collected Abstract of Powder Diffraction Meeting (Toulouse), 1990, p. 127) and integrated in WinPlotr (T. Roisnel, J. Rodriguez-Carvajal, Mater. Sci. Forum 2001, 378-381, 118-123). CCDC-194049 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge vía www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Center, 12, Union Road, Cambridge CB21EZ, UK; fax: (+44)1223-336-033; or deposit@ccdc.cam.ac.uk).
    • (1990) Collected Abstract of Powder Diffraction Meeting , pp. 127
    • Rodriguez-Carvajal, J.1
  • 27
    • 0035184477 scopus 로고    scopus 로고
    • High-resolution synchrotron data were measured with a Debye-Scherrer diffractometer geometry and a Si(111) analyzer crystal (λ = 0.7999 Å). The powder was introduced in a 1.5 mm capillary and the pattern was scanned in the range 2 θ = 1-60° with a step length of 2 θ = 0.0035° and a counting time of 1 s per step. To improve the counting statistics at high angles, the pattern was then divided in two 2 θ regions (1-15 and 15-45°), with times per step of 1 and 3 s, respectively. Pattern indexing was carried out with DICVOL91 (A. Boultif, D. Louër, J. Appl. Crystallogr. 1991, 24, 987-993). Direct methods and Fourier difference calculations were performed with SHELXTL (G. M. Sheldrick, 1997). Pattern matching and Rietveld refinements were performed by using FullProf (J. Rodriguez-Carvajal in Collected Abstract of Powder Diffraction Meeting (Toulouse), 1990, p. 127) and integrated in WinPlotr (T. Roisnel, J. Rodriguez-Carvajal, Mater. Sci. Forum 2001, 378-381, 118-123). CCDC-194049 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge vía www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Center, 12, Union Road, Cambridge CB21EZ, UK; fax: (+44)1223-336-033; or deposit@ccdc.cam.ac.uk).
    • (2001) Mater Sci Forum , vol.378-381 , pp. 118-123
    • Roisnel, T.1    Rodriguez-Carvajal, J.2
  • 30
    • 0013393705 scopus 로고    scopus 로고
    • note
    • -1).
  • 31
    • 0013389897 scopus 로고    scopus 로고
    • note
    • The BET surface area of the sample activated at 170°C under vacuum for 64 h was studied on a Micromeritics ASP200 porosimeter.
  • 32
    • 0013344649 scopus 로고    scopus 로고
    • note
    • Magnetization measurements were performed on a Quantum Design Squid magnetometer (MPMS-5).
  • 40
    • 0035805105 scopus 로고    scopus 로고
    • a) K. D. M. Harris, M. Tremayne, B. M. Kariuki, Angew. Chem. 2001, 113, 1674-1700; Angew. Chem. Int. Ed. 2001, 40, 1626-1651;
    • (2001) Angew. Chem. Int. Ed. , vol.40 , pp. 1626-1651
  • 42
    • 0034671893 scopus 로고    scopus 로고
    • b) E. Tedesco, G. W. Turner, K. D. M. Harris, R. L. Johnston, B. M. Kariuki, Angew. Chem. 2000, 112, 4662-4665; Angew. Chem. Int. Ed. 2000, 39, 4488-4491;
    • (2000) Angew. Chem. Int. Ed. , vol.39 , pp. 4488-4491
  • 44
    • 0036470786 scopus 로고    scopus 로고
    • c) E. Y. Cheung, E. E. McCabe, K. D. M. Harris, R. L. Johnston, E. Tedesco, K. M. P. Raja, P. Balaram, Angew. Chem. 2002, 114, 512-514; Angew. Chem. Int. Ed. 2002, 41, 494-496;
    • (2002) Angew. Chem. Int. Ed. , vol.41 , pp. 494-496


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.