Solvothermal synthesis and structure of anhydrous manganese(II) formate, and its topotactic dehydration from manganese(II) formate dihydrate

European Journal of Inorganic Chemistry

Volumn , Issue 12, 2003, Pages 2283-2289

  Viertelhaus, Martin ^a   Henke, Henning ^a   Anson, Christopher E ^a   Powell, Annie K ^a  

^a UNIVERSITY OF KARLSRUHE   (Germany)

Author keywords

Formates; Manganese; Solid state reactions; Solvothermal synthesis

Indexed keywords

CRYSTAL STRUCTURE; DEHYDRATION; MANGANESE COMPOUNDS; SINGLE CRYSTALS; X RAY DIFFRACTION;

CRYSTAL STRUCTURE DETERMINATION; FORMATE; FORMATE DIHYDRATE; RECRYSTALLISATION; SINGLE-CRYSTAL STRUCTURE; SOLID-STATE REACTIONS; SOLVOTHERMAL CONDITIONS; SOLVOTHERMAL SYNTHESIS; STRUCTURAL RELATIONSHIP; X- RAY DIFFRACTIONS;

SOLID STATE REACTIONS;

FORMIC ACID DERIVATIVE; MANGANESE DERIVATIVE; MANGANESE FORMATE; METAL COMPLEX; UNCLASSIFIED DRUG;

ARTICLE; CRYSTAL STRUCTURE; CRYSTALLIZATION; DEHYDRATION; SOLID STATE; STRUCTURE ANALYSIS; SYNTHESIS; X RAY DIFFRACTION;

EID: 0037929147     PISSN: 14341948     EISSN: None     Source Type: Journal    
DOI: 10.1002/ejic.200200699     Document Type: Article

References (43)

1. R. D. Cannon, R. P. White, Prog. Inorg. Chem. 1988, 36, 195-298.
2. T. Lis, Acta Crystallogr., Sect. B 1980, 2042-2046.
3. [3a] H. J. Eppley, H.-L. Tsai, N. de Vires, K. Folting, G. Christou, D. N. Hendrikson, J. Am. Chem. Soc. 1995, 117, 301-317.
4. [3b] S. M. J. Aubin, Z. Sun, I. A. Guzei, A. L. Rheingold, G. Christou, D. N. Hendrikson, Chem. Commun. 1997, 2239-2240.
5. [4a] Z. A. D. Lethbridge, A. D. Hiller, R. Cywinski, P. Lightfoot, Dalton Trans. 2000, 1595-1599.
6. [4b] P. A. Prasad, S. Neeraj, S. Natarajan, C. N. R. Rao, Chem. Commun. 2000, 1251-1252.
7. [4c] Z. A. D. Lethbridge, S. K. Tiwary, A. Harrison, P. Lightfoot, Dalton Trans. 2001, 1904-1910.
8. J. D. Martin, R. F. Hess, Chem. Commun. 1996, 2419-2420.
9. G. A. Tikhomirov, K. O. Znamenkov, I. V. Morozov, E. Kemnitz, S. I. Troyanov, Zeitschr. Anorg. Allg Chem. 2002, 28, 296-273.
10. R. W. G. Wyckoff, American Journal of Science 1920, 50, 317-360.
11. J. L. Galigné, Acta Crystallogr., Sect. B 1971, 2429-2431.
12. K. Osaki, Y. Nakai, T. Watanabe, J. Phys. Soc. Jap. 1963, 18, 919.
13. D. Stoilova, St. Peter, H. D. Lutz, Zeitschr Anorg. Allg. Chem. 1994, 620, 1793-1798.
14. F. Sapina, M. Burgos, E. Escrivá, J.-V. Folgado, D. Marcos, A. Beltrán, D. Beltrán, Inorg. Chem. 1993, 32, 4337-4344.
15. G. Weber, Actc Cryst. Sect. B 1980, 1947-1949.
16. E. Kalalova, V. Ruzicka, Coll. Czech. Chem. Commun. 1962, 27, 424-429.
17. [14a] R. C. Eckhardt, P. M. Fichte, T. B. Flanagan, Trans. Faraday. Soc. 1971, 67, 1143-1154.
18. [14b] Y. Masuda, M. Hatakeyama, Talanta 1996, 43, 1705-1709.
19. [14c] Y. Masuda, M. Hatakeyama, Thermochim. Acta 1998, 308, 165-170.
20. D. Dollimore, J. P. Gupta, D. V. Nowell, Thermochim. Acta 1979, 30, 339-350.
21. R. C. Eckhardt, T. B. Flanagan, Trans. Faraday Soc 1964, 60, 1289-1298.
22. C. Malard, C. R. Acad. Sc. Paris Ser. C 1966, 263, 480-483.
23. T. Arii, A. Kishi, Y. Kobayashi, Thermochim. Acta 1999, 325, 151-156.
24. G. Périnet, Bull. Soc. franc. Minér Crist. 1966, 89, 325-328.
25. T. Arii, A. Kishi, Thermochim. Acta 1999, 325, 157-165.
26. V. Z. Vassileva, A. L. Karapetkova, Bulg. Chem. Commun. 1995, 28, 151-159.
27. G. Weber, Zeitschr. f. Krist. 1982, 158, 315-318.
28. B. Krebs, Angew. Chem. 1969, 81, 120; Angew. Chem. Int. Ed. Engl. 1969, 8, 146-147.
29. B. Krebs, Angew. Chem. 1969, 81, 120; Angew. Chem. Int. Ed. Engl. 1969, 8, 146-147.
30. M. Elder, B. R. Penfold, Inorg. Chem. 1966, 5, 1197-1200.
31. [25a] U. Dahmen, M. G. Kim, A. W. Searcy, Ultramicroscopy 1987, 23, 365-370.
32. [25b] J. Lima-de-Faria, Acta Crystallogr. 1967, 23, 733-736.
33. P. Baraldi, Spectrochim. Acta 1979, 35A, 1003-1007.
34. J. D. Donaldson, J. F. Knifton, S. D. Ross, Spectrochim. Acta 1964, 20, 847-51.
35. [28a] P. Burlet, P. Burlet, J. Rossat-Mignod, A. de Combarieu, E. Bedin, Phys. Stat. Sol. 1975, 71, 675-685.
36. [28b] P. Radhakrishna, B. Gillon, G. Chevier, J. Phys.: Condens. Matter 1993, 5, 6447-60.
37. [29a] G. S. Papaefstathiou, R. Vicente, C. P. Raptopoulou, A. Terzis, A. Escuer, S. P. Perlepes, Eur. J. Inorg. Chem. 2002, 2488-2493.
38. [29b] G. Aromi, P. C. Berzal, P. Cames, O. Roubeau, H. Kooijman, A. L. Spek, W. L. Driessen, J. Reedijk, Angew. Chem. 2001, 113, 3552-3554; Angew. Chem. Int. Ed. 2001, 40, 3444-3446.
39. [29b] G. Aromi, P. C. Berzal, P. Cames, O. Roubeau, H. Kooijman, A. L. Spek, W. L. Driessen, J. Reedijk, Angew. Chem. 2001, 113, 3552-3554; Angew. Chem. Int. Ed. 2001, 40, 3444-3446.
40. [29c] M. D. Carducci, R. J. Doedens;, Inorg. Chem. 1989, 28, 2492-2494.
41. V. Tangoulis, G. Psomas, C. Dendrinou-Samara, C. P. Raptopoulou, A. Terzis, D. P. Kessissoglou, Inorg. Chem. 1996, 35, 7655-7660.
42. G. M. Sheldrick, SHELXTL 5.1, Bruker AXS Inc., Madison, WI, 1997.
43. B. Anselment, Dissertation, Universität Karlsruhe, 1986.