Determination of water self-diffusion coefficient in complex food products by low field 1H PFG-NMR: Comparison between the standard spin-echo sequence and the T1-weighted spin-echo sequence

Journal of Magnetic Resonance

Volumn 165, Issue 2, 2003, Pages 265-275

  Métais, Angélique ^a   Mariette, François ^a  

^a CEMAGREF   (France)

Author keywords

1H NMR; Food products; Low field NMR; Relaxation; Self diffusion

Indexed keywords

DIFFUSION; EMULSIONS; NUCLEAR MAGNETIC RESONANCE; OILS AND FATS; PROTEINS; WATER;

SELF-DIFFUSION COEFFICIENT; SPIN-ECHO SEQUENCES;

FOOD PRODUCTS;

GLYCOLIPID; GLYCOPROTEIN; MILK PROTEIN; WATER;

ANIMAL; ARTICLE; CATTLE; CHEESE; CHEMISTRY; COMPARATIVE STUDY; DIFFUSION; EMULSION; EVALUATION; FOOD ANALYSIS; METHODOLOGY; MILK; MILK FAT GLOBULE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; SIGNAL PROCESSING; VALIDATION STUDY;

ANIMALS; CATTLE; CHEESE; DIFFUSION; EMULSIONS; FOOD ANALYSIS; GLYCOLIPIDS; GLYCOPROTEINS; MAGNETIC RESONANCE SPECTROSCOPY; MILK; MILK PROTEINS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SIGNAL PROCESSING, COMPUTER-ASSISTED; WATER;

EID: 0344896552     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jmr.2003.09.001     Document Type: Article

References (27)

1. Stilbs P. Fourier transform pulsed-gradient spin-echo studies of molecular diffusion. Prog. NMR Spectrosc. 19:1987;1-45.
2. Kärger J., Pfeiffer H., Heink W. Principles and application of self-diffusion measurements by nuclear magnetic resonance. Adv. Magn. Reson. 12:1988;1-89.
3. Price W.S. Pulsed field gradient nuclear magnetic resonance as a tool for studying translational diffusion: Part 1. Basic theory. Concepts Magn. Reson. 9:1997;299-336.
4. Ohtsuka A., Watanabe T., Suzuki T. Gel structure and water diffusion phenomena in starch gels studied by pulsed field gradient stimulated echo NMR. Carbohydr. Polym. 25:1994;95-100.
5. Callaghan P.T., Jolley K.W., Lelievre J., Wong R.B.K. Nuclear magnetic resonance studies of wheat starch pastes. J. Colloid Interface Sci. 92:1983;332-337.
6. Umbach S.L., Davis E.A., Gordon J., Callaghan P.T. Water self-diffusion coefficients and dielectric properties determined for starch-gluten-water mixtures heated by microwave and by conventional methods. Cereal Chem. 69:1992;637-642.
7. Ohtsuka A., Watanabe T. The network structure of gellan gum hydrogels based on the structural parameters by the analysis of the restricted diffusion of water. Carbohydr. Polym. 30:1996;135-140.
8. Callaghan P.T., Jolley K.W., Humphrey R.S. Diffusion of fat and water in cheese as studied by pulsed field gradient nuclear magnetic resonance. J. Colloid Interface Sci. 93:1983;521-529.
9. Roudaut G., van Dusschoten D., Van As H., Hemminga M.A., Le Meste M. Mobility of lipids in low moisture bread as studied by NMR. J. Cereal Sci. 28:1998;147-155.
10. Lindman B., Ölsson U., Söderman O. Characterization of microemulsions by NMR. Kumar P., Mittal K.L. Handbook of Microemulsion Science and Technology. 1999;309-356 Marcel Dekker, New York.
11. Stejskal E.O., Tanner J.E. Spin diffusion measurements: Spin echoes in the presence of time-dependent field gradient. J. Chem. Phys. 42:1965;288-292.
12. Ambrosone L., Ceglie A., Colafemmina G., Palazzo G. Resolving complex mixtures by means of pulsed gradient spin- echo NMR experiments. Phys. Chem. Chem. Phys. 4:2002;3040-3047.
13. Antalek B. Using pulsed gradient spin echo NMR for chemical mixture analysis: How to obtain optimum results. Concepts Magn. Reson. 14:2002;225-258.
14. Van Duynhoven J.P.M., Goudappel G.J.W., van Dalen G., van Bruggen P.C., Blonk J.C.G., Eijkelenboom A.P.A.M. Scope of droplet size measurements in food emulsions by pulsed field gradient NMR at low field. Magn. Reson. Chem. 40:2002;S51-S59.
15. Hills B.P., Godward J., Manning C.E., Biechlin J.L., Wright K.M. Microstructural characterization of starch systems by NMR relaxation and Q-SPACE microscopy. Magn. Reson. Imaging. 16:1998;557-564.
16. Farhat I.A., Loisel E., Saez P., Derbyshire W., Blanshard J.M.V. The effect of sugars on the diffusion of water in starch gels: a pulsed field gradient NMR study. Int. J. Food Sci. Technol. 32:1997;377-387.
17. van Dusschoten D., de Jager P.A., Van As H. Extracting diffusion constants from echo-time-dependent PFG NMR data using relaxation-time information. J. Magn. Reson. A. 116:1995;22-28.
18. van Dusschoten D., de Jager P.A., Van As H. Flexible PFG NMR desensitized for susceptibility artifacts, using the PFG multiple-spin-echo sequence. J. Magn. Reson. A. 112:1995;237-240.
19. Van Den Enden J.C., Waddington D., Van Aalst H., Van Kralingen C.G., Packer K.J. Rapid determination of water droplet size distributions by PFG-NMR. J. Colloid Interface Sci. 140:1990;105-113.
20. Hills B.P., Manoj P., Destruel C. NMR Q-space microscopy of concentrated oil-in-water emulsions. Magn. Reson. Imaging. 18:2000;319-333.
21. Marquardt D.W. An algorithm for least squares estimations of nonlinear parameters. J. Soc. Industr. Appl. Math. 11:1963;431.
22. Mariette F., Guillement J.P., Tellier C., Marchal P. Continuous relaxation time distribution decomposition by MEM. Rutledge D.N. Signal Treatment and Signal Analysis in NMR. 1996;218-234 Elsevier, Paris.
23. Le Dean A. Caractérisation de l'eau dans les produits laitiers: Cas des dispersions et des gels égoutés et congelés. 2000;Institut National Agronomique Paris-Grignon, Paris. pp. 184.
24. Le Botlan D.J., Helie I. A novel approach to the analysis of fats by low resolution NMR spectroscopy: application to milk and vegetable fats. Analysis. 22:1994;108-113.
25. Chaland B., Mariette F., Marchal P., de Certaines J. H1 nuclear magnetic resonance relaxometric characterization of fat and water states in soft and hard cheese. J. Dairy Res. 67:2000;609-618.
26. 1H NMR diffusometry study of water in casein dispersion and gels. J. Agric. Food Chem. 50:2002;4295-4302.
27. Topgaard D., Söderman O. Self-diffusion on two and three-dimensional powders of anisotropic domains: an NMR study of the diffusion of water in cellulose and starch. J. Phys. Chem. 106:2002;11887-11892.