Separation of selected bile acids by TLC. I

Journal of Liquid Chromatography and Related Technologies

Volumn 26, Issue 7, 2003, Pages 1095-1108

  Pyka, A ^a   Dolowy M ^a  

^a MEDICAL UNIVERSITY OF SILESIA   (Poland)

Author keywords

Bile acids; TLC

Indexed keywords

ALUMINUM; COMPOSITION; SEPARATION; SILICA GEL;

BILE ACIDS;

CARBOXYLIC ACIDS;

ACETIC ACID; ACETIC ACID ETHYL ESTER; ALUMINUM DERIVATIVE; BILE ACID; CHENODEOXYCHOLIC ACID; CHOLIC ACID; DEOXYCHOLIC ACID; GLYCOCHOLIC ACID; GLYCODEOXYCHOLIC ACID; GLYCOLITHOCHOLIC ACID; HEPTANE; LITHOCHOLIC ACID; SILICA GEL;

ANALYTIC METHOD; ARTICLE; CHEMICAL ANALYSIS; CHEMICAL COMPOSITION; MATHEMATICAL ANALYSIS; SEPARATION TECHNIQUE; THIN LAYER CHROMATOGRAPHY;

EID: 0242432351     PISSN: 10826076     EISSN: None     Source Type: Journal    
DOI: 10.1081/JLC-120020096     Document Type: Article

References (26)

1. Murray, R.K.; Granner, D.K.; Mayes, P.A.; Rodwell, V.W. Harper's Biochemistry (Biochemia Harpera) (in Polish); Wydawnictwo Lekarskie PZWL: Warsaw, 1995.
2. Bunya, M.; Maebuchi, M.; Kamiryo, T; Kurosawa, T.; Sato, M.; Tohma, M.; Jiang, L.L.; Hashimoto, T. Thiolase involved in bile acid formation. J. Biochem. (Tokyo) 1998, 123 (2), 347-352.
3. Sauter, G.; Fischer, S.; Pahemik, S.; Koebe, H.G.; Paumgartner, G. Formation of cholic acid and chenodeoxycholic acid from 7 alphahydroxycholesterol and 27-hydroxycholesterol by primary cultures of human hepatocytes. Biochim. Biophys. Acta 1996, 1300 (1), 25-29.
4. Axelson, M.; Ellis, E.; Mork, B.; Garmark, K.; Abrahamsson, A.; Bjorkhem, I.; Ericzon, B.G.; Einarsson, C. Bile acid synthesis in cultured human hepatocytes: support for an alternative biosynthetic pathway to cholic acid. Hepatology 2000, 31 (6), 1305-1312.
5. Nakayama, F. Quantitative microanalysis of bile acids in biological samples. Collaborative study. J. Chromatogr. 1988, 452, 399-408.
6. Caderni, G.; Stuart, E.; Anderson, A.M.; Bruce, W.R. A CHO cell line resistant to deoxycholic acid. Cancer Lett. 1987, 38 (1-2), 119-127.
7. Fedorowski, T.; Salen, G.; Tint, G.S.; Mosbach, E. Transformation of chenodeoxycholic acid and ursodeoxycholic acid by human intestinal bacteria. Gastroenterology 1979, 77 (5), 1068-1073.
8. Salen, G.; Tint, G.S.; Eliav, B.; Deering, N.; Mosbach, E.H. Increased formation of ursodeoxycholic acid in patients treated with chenodeoxycholic acid. J. Clin. Invest. 1974, 53 (2), 612-621.
9. Rodrigues, C.M.; Brites, D.; Serejo, F.; Costa, A.; Ramalho, F.; De Moura, M.C. Apoptotic cell death does not parallel other indicators of liver damage in chronic hepatitis C patients. J. Viral Hepat. 2000, 7 (3), 175-183.
10. Fracchia, M.; Pellegrino, S.; Secreto, P.; Calgaro, M.; Taraglio, S.; Pera, A.; Galatola, G. Biliary bile acid composition in gastric cancer. Int. J. Clin. Lab. Res. 1999, 29 (1), 46-48.
11. Mamianetti, A.; Garrido, D.; Carducci, C.N.; Vescina, M.C. Fecal bile acid excretion profile in gallstone patients. Medicina (B-Aires) 1999, 59 (3), 269-273.
12. Halvorsen, B.; Kase, B.F.; Prydz, K.; Garagozlian, S.; Andresen, M.S.; Kolset, S.O. Sulphation of lithocholic acid in the colon-carcinoma cell line CaCo-2. Biochem. J. 1999, 343, 3533-3539.
13. Charach, G.; Rabinovich, P.D.; Konikoff, F.M.; Grosskopf, I.; Weintraub, M.S.; Gilat, T. Decreased fecal bile acid output in patients with coronary atherosclerosis. J. Med. 1998, 29 (3-4), 125-136.
14. Kishida, T.; Taguchi, F.; Feng, L.; Tatsuguchi, A.; Sato, J.; Fujimori, S.; Tachikawa, H.; Tamagawa, Y.; Yoshida, Y.; Kobayashi, M. Analysis of bile acids in colon residual liquid or fecal material in patients with colorectal neoplasia and control subjects. J. Gastroenterol. 1997, 32 (3), 306-311.
15. Boehm, G.; Braun, W.; Moro, G.; Minoli, I. Bile acid concentrations in serum and duodenal aspirates of healthy preterm infants: effects of gestational and postnatal age. Biol. Neonate. 1997, 71 (4), 207-214.
16. Fischer, S.; Beuers, U.; Spengler, U.; Zwiebel, EM.; Koebe, H.G. Hepatic levels of bile acids in end-stage chronic cholestatic liver disease. Clin. Chim. Acta 1996, 251 (2), 173-186.
17. Wells, J.E.; Berr, F.; Thomas, L.A.; Dowling, R.H.; Hylemon, P.B. Isolation and characterization of cholic acid 7alpha-dehydroxylating fecal bacteria from cholesterol gallstone patients. J. Hepatol. 2000, 32 (1), 4-10.
18. Kimura, A.; Mahara, R.; Inoue, T.; Nomura, Y.; Murai, T.; Kurosawa, T.; Tohma, M.; Noguchi, K.; Hoshiyama, A.; Fujisawa, T.; Kato, H. Profile of urinary bile acids in infants and children: developmental pattern of excretion of unsaturated ketonic bile acids and 7beta-hydroxylated bile acids. Pediatr. Res. 1999, 45 (4), 603-609.
19. Thomas, L.A.; Veysey, M.J.; Bathgate, T.; King, A.; French, G.; Smeeton, N.C.; Murphy, G.M.; Dowling, R.H. Mechanism for the transit-induced increase in colonic deoxycholic acid formation in cholesterol cholelithiasis. Gastroenterology 2000, 119 (3), 806-815.
20. Ochsenkuhn, T.; Bayerdorffer, E.; Meining, A.; Schinkel, M.; Thiede, C.; Nussler, V.; Sackmann, M.; Hatz, R.; Neubauer, A.; Paumgartner, G. Colonic mucosal proliferation is related to serum deoxycholic acid levels. Cancer 1999, 85 (8), 1664-1669.
21. Kauer, W.K.; Peters, J.H.; DeMeester, T.R.; Feussner, H.; Ireland, A.P.; Stein, H.J.; Siewert, R.J. Composition and concentration of bile acid reflux into the esophagus of patients with gastroesophageal reflux disease. Surgery 1997, 122 (5), 874-881.
22. Fein, M.; Fuchs, K.H.; Stopper, H.; Diem, S.; Herderich, M. Duodenogastric reflux and foregut carcinogenesis: analysis of duodenal juice in a rodent model of cancer. Carcinogenesis 2000, 21 (11), 2079-2084.
23. Lepri, L.; Cincinelli, A.; Del Bubba, M. Reversed phase planar chromatography of optical isomers on microcrystalline cellulose triacetate. J. Planar Chromatogr.-Modern TLC 1999, 12 (4), 298-301.
24. Sliwiok, J.; Kwapniewski, Z. Regularity of process of chromatographic separation of homologous series of higher fatty acids (in Polish). Pedagogical University in Katowice, Scientific book, Section of Chemistry 1963, 4, 47-50.
25. Sliwiok, J. Influence of the mobile and stationary phases on the RF values of the fatty acids in paper chromatography (in Polish). Pedagogical University in Katowice, Scientific book, Section of Chemistry 1965, 5, 65-72.
26. Szepesi, G.; Dudas, K.; Vegh, Z.; Mincsovics, E.; Tyihak, T. Quantitative analysis of chenodeoxycholic acid and related compounds by a densitometric thin-layer chromatographic method. J. Chromatogr. 1982, 237, 137-143.