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The desired aldehyde was obtained in 35% together with 5 in 3%, under usual conditions. In order to minimize the formation of the coupling products, slow addition of 4 to the reaction medium was examined, but the yield of the desired aldehyde was insufficient and irreproducible (27-67%), see: (a) Irie, R.; Noda, K.; Ito, Y.; Matsumoto, N.; Katsuki, T. Tetrahedron Lett. 1990, 31, 7345. (b) Irie, R.; Noda, K.; Ito, Y.; Matsumoto, N.; Katsuki, T. Tetrahedron: Asymmetry 1991, 2, 481.
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The desired aldehyde was obtained in 35% together with 5 in 3%, under usual conditions. In order to minimize the formation of the coupling products, slow addition of 4 to the reaction medium was examined, but the yield of the desired aldehyde was insufficient and irreproducible (27-67%), see: (a) Irie, R.; Noda, K.; Ito, Y.; Matsumoto, N.; Katsuki, T. Tetrahedron Lett. 1990, 31, 7345. (b) Irie, R.; Noda, K.; Ito, Y.; Matsumoto, N.; Katsuki, T. Tetrahedron: Asymmetry 1991, 2, 481.
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0142070073
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note
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13b).
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