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Volumn 165, Issue 1, 2003, Pages 102-115

PFG-assisted selection and suppression of 1H NMR signals in the solid state under fast MAS

Author keywords

Fast MAS; Peak selection; Peak suppression; Pulsed field gradients; Solid state 1H NMR

Indexed keywords

FOURIER TRANSFORMS; MAGNETIZATION; SIGNAL PROCESSING;

EID: 0142043436     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jmr.2003.07.002     Document Type: Article
Times cited : (13)

References (60)
  • 1
    • 0000677728 scopus 로고
    • Selective excitation in high-resolution NMR
    • Freeman R. Selective excitation in high-resolution NMR. Chem. Rev. 91:1991;1397-1412.
    • (1991) Chem. Rev. , vol.91 , pp. 1397-1412
    • Freeman, R.1
  • 2
    • 0002812449 scopus 로고
    • High resolution NMR using selective excitation
    • Freeman R. High resolution NMR using selective excitation. J. Mol. Struct. 266:1992;39-51.
    • (1992) J. Mol. Struct. , vol.266 , pp. 39-51
    • Freeman, R.1
  • 3
    • 43949166518 scopus 로고
    • Techniques for multisite excitation
    • Kupce E., Freeman R. Techniques for multisite excitation. J. Magn. Reson. A. 105:1993;234-238.
    • (1993) J. Magn. Reson. A , vol.105 , pp. 234-238
    • Kupce, E.1    Freeman, R.2
  • 4
    • 0037598366 scopus 로고
    • Polychromatic selective pulses
    • Kupce E., Freeman R. Polychromatic selective pulses. J. Magn. Reson. A. 102:1993;122-126.
    • (1993) J. Magn. Reson. A , vol.102 , pp. 122-126
    • Kupce, E.1    Freeman, R.2
  • 5
    • 48749149745 scopus 로고
    • Solvent suppression in Fourier transform nuclear magnetic resonance
    • Hore P.J. Solvent suppression in Fourier transform nuclear magnetic resonance. J. Magn. Reson. 55:1983;283-300.
    • (1983) J. Magn. Reson. , vol.55 , pp. 283-300
    • Hore, P.J.1
  • 8
    • 44949280676 scopus 로고
    • Band-selective radiofrequency pulses
    • Geen H., Freeman R. Band-selective radiofrequency pulses. J. Magn. Reson. 93:1991;93-141.
    • (1991) J. Magn. Reson. , vol.93 , pp. 93-141
    • Geen, H.1    Freeman, R.2
  • 9
    • 0031144788 scopus 로고    scopus 로고
    • NMR techniques employing selective radiofrequency pulses in combination with pulsed field gradients
    • Berger S. NMR techniques employing selective radiofrequency pulses in combination with pulsed field gradients. Progr. Nucl. Magn. Reson. Spectr. 30:1997;137-156.
    • (1997) Progr. Nucl. Magn. Reson. Spectr. , vol.30 , pp. 137-156
    • Berger, S.1
  • 10
    • 0347722841 scopus 로고    scopus 로고
    • Heteronuclear multidimensional NMR experiments for the structure determination of proteins in solution employing pulsed field gradients
    • Sattler M., Schleucher J., Griesinger C. Heteronuclear multidimensional NMR experiments for the structure determination of proteins in solution employing pulsed field gradients. Progr. NMR Spectr. 34:1999;93-158.
    • (1999) Progr. NMR Spectr. , vol.34 , pp. 93-158
    • Sattler, M.1    Schleucher, J.2    Griesinger, C.3
  • 11
    • 84989011375 scopus 로고
    • High-resolution NMR experiments which use frequency-selective RF pulses in combination with magnetic-field gradients
    • Bernstein M.A., Trimble L.A. High-resolution NMR experiments which use frequency-selective RF pulses in combination with magnetic-field gradients. Magn. Reson. Chem. 32:1994;107-110.
    • (1994) Magn. Reson. Chem. , vol.32 , pp. 107-110
    • Bernstein, M.A.1    Trimble, L.A.2
  • 12
    • 0000480074 scopus 로고
    • 1-2-1 pulse train: A new effective method of selective excitation for proton NMR in water
    • Sklenar V., Starcuk Z. 1-2-1 pulse train: a new effective method of selective excitation for proton NMR in water. J. Magn. Reson. 50:1982;495-501.
    • (1982) J. Magn. Reson. , vol.50 , pp. 495-501
    • Sklenar, V.1    Starcuk, Z.2
  • 14
    • 0000224420 scopus 로고
    • Simple pulse sequence for selective excitation in Fourier-transform NMR
    • Bodenhausen G., Freeman R., Morris G.A. Simple pulse sequence for selective excitation in Fourier-transform NMR. J. Magn. Reson. 23:1976;171-175.
    • (1976) J. Magn. Reson. , vol.23 , pp. 171-175
    • Bodenhausen, G.1    Freeman, R.2    Morris, G.A.3
  • 16
    • 0026951903 scopus 로고
    • Gradient-tailored excitation for single-quantum NMR spectroscopy of aqueous solutions
    • Piotto M., Saudek V., Sklenar V. Gradient-tailored excitation for single-quantum NMR spectroscopy of aqueous solutions. J. Biomol. NMR. 2:1992;661-665.
    • (1992) J. Biomol. NMR , vol.2 , pp. 661-665
    • Piotto, M.1    Saudek, V.2    Sklenar, V.3
  • 18
    • 0000842595 scopus 로고
    • Binomial solvent suppression
    • Turner D. Binomial solvent suppression. J. Magn. Reson. 54:1983;146-148.
    • (1983) J. Magn. Reson. , vol.54 , pp. 146-148
    • Turner, D.1
  • 20
    • 0142039278 scopus 로고
    • NMR spectra of exchangeable protons using uniform excitation solvent suppression pulse sequences
    • Wang C., Pardi A. NMR spectra of exchangeable protons using uniform excitation solvent suppression pulse sequences. J. Magn. Reson. 71:1987;154-158.
    • (1987) J. Magn. Reson. , vol.71 , pp. 154-158
    • Wang, C.1    Pardi, A.2
  • 21
    • 0003052693 scopus 로고    scopus 로고
    • Shaped radiofrequency pulses in high resolution NMR
    • Freeman R. Shaped radiofrequency pulses in high resolution NMR. Progr. Nucl. Magn. Reson. Spectr. 32:1998;59-106.
    • (1998) Progr. Nucl. Magn. Reson. Spectr. , vol.32 , pp. 59-106
    • Freeman, R.1
  • 22
    • 0028673795 scopus 로고
    • Selective pulses and their applications to assignment and structure determination in nuclear magnetic resonance
    • Emsley L. Selective pulses and their applications to assignment and structure determination in nuclear magnetic resonance. Method Enzymol. 239:1994;207-246.
    • (1994) Method Enzymol. , vol.239 , pp. 207-246
    • Emsley, L.1
  • 23
    • 0036298982 scopus 로고    scopus 로고
    • Adjustable, broadband, selective excitation with uniform phase
    • Cano K.E., Smith M.A., Shaka A.J. Adjustable, broadband, selective excitation with uniform phase. J. Magn. Reson. 155:2002;131-139.
    • (2002) J. Magn. Reson. , vol.155 , pp. 131-139
    • Cano, K.E.1    Smith, M.A.2    Shaka, A.J.3
  • 25
    • 0031578999 scopus 로고    scopus 로고
    • Pulsed field gradient multiple quantum MAS NMR spectroscopy of half-integer spin quadrupolar nuclei
    • Fyfe C.A., Skibsted J., Grondey H., Meyer H. Pulsed field gradient multiple quantum MAS NMR spectroscopy of half-integer spin quadrupolar nuclei. Chem. Phys. Lett. 281:1998;44.
    • (1998) Chem. Phys. Lett. , vol.281 , pp. 44
    • Fyfe, C.A.1    Skibsted, J.2    Grondey, H.3    Meyer, H.4
  • 27
    • 0001048159 scopus 로고    scopus 로고
    • Pulsed field gradient selection in two-dimensional magic angle spinning NMR spectroscopy of dipolar solids
    • Fritzhanns T., Hafner S., Demco D.E., Spiess H.W., Laukien F.H. Pulsed field gradient selection in two-dimensional magic angle spinning NMR spectroscopy of dipolar solids. J. Magn. Reson. 134:1998;355-359.
    • (1998) J. Magn. Reson. , vol.134 , pp. 355-359
    • Fritzhanns, T.1    Hafner, S.2    Demco, D.E.3    Spiess, H.W.4    Laukien, F.H.5
  • 28
    • 0030869479 scopus 로고    scopus 로고
    • High-resolution NMR techniques for solid-phase synthesis and combinatorial chemistry
    • Keifer P.A. High-resolution NMR techniques for solid-phase synthesis and combinatorial chemistry. Drug Discovery Today. 2:1997;468-478.
    • (1997) Drug Discovery Today , vol.2 , pp. 468-478
    • Keifer, P.A.1
  • 31
    • 0030659813 scopus 로고    scopus 로고
    • Magic angle spinning nuclear magnetic resonance in solid-phase peptide synthesis
    • Dhalluin C., Boutillon C., Tartar A., Lippens G. Magic angle spinning nuclear magnetic resonance in solid-phase peptide synthesis. J. Am. Chem. Soc. 119:1997;10494.
    • (1997) J. Am. Chem. Soc. , vol.119 , pp. 10494
    • Dhalluin, C.1    Boutillon, C.2    Tartar, A.3    Lippens, G.4
  • 32
    • 0034052957 scopus 로고    scopus 로고
    • High-resolution magic angle spinning NMR study of resin-bound polyalanine peptides
    • Warrass R., Wieruszeski J.M., Boutillon C., Lippens G. High-resolution magic angle spinning NMR study of resin-bound polyalanine peptides. J. Am. Chem. Soc. 122:2000;1789.
    • (2000) J. Am. Chem. Soc. , vol.122 , pp. 1789
    • Warrass, R.1    Wieruszeski, J.M.2    Boutillon, C.3    Lippens, G.4
  • 33
    • 0034806251 scopus 로고    scopus 로고
    • Evidence of secondary structure by high-resolution magic angle spinning NMR spectroscopy of a bioactive peptide bound to different solid supports
    • Furrer J., Piotto M., Bourdonneau M., Limal D., Guichard G., Elbayed K., Raya J., Briand J.P., Bianco A.J. Evidence of secondary structure by high-resolution magic angle spinning NMR spectroscopy of a bioactive peptide bound to different solid supports. J. Am. Chem. Soc. 123:2001;4130.
    • (2001) J. Am. Chem. Soc. , vol.123 , pp. 4130
    • Furrer, J.1    Piotto, M.2    Bourdonneau, M.3    Limal, D.4    Guichard, G.5    Elbayed, K.6    Raya, J.7    Briand, J.P.8    Bianco, A.J.9
  • 34
    • 0030449483 scopus 로고    scopus 로고
    • Gradient, high-resolution, magic-angle sample spinning NMR
    • Maas W.E., Laukien F.H., Cory D.G. Gradient, high-resolution, magic-angle sample spinning NMR. J. Am. Chem. Soc. 118:1996;13085-13086.
    • (1996) J. Am. Chem. Soc. , vol.118 , pp. 13085-13086
    • Maas, W.E.1    Laukien, F.H.2    Cory, D.G.3
  • 35
    • 45149145322 scopus 로고
    • Rotational-echo double-resonance NMR
    • Gullion T., Schaefer J. Rotational-echo double-resonance NMR. J. Magn. Reson. 81:1989;196-200.
    • (1989) J. Magn. Reson. , vol.81 , pp. 196-200
    • Gullion, T.1    Schaefer, J.2
  • 36
    • 85011817347 scopus 로고
    • Detection of weak heteronuclear dipolar coupling by rotational-echo double-resonance nuclear magnetic resonance
    • Gullion T., Schaefer J. Detection of weak heteronuclear dipolar coupling by rotational-echo double-resonance nuclear magnetic resonance. Adv. Magn. Reson. 13:1989;57-83.
    • (1989) Adv. Magn. Reson. , vol.13 , pp. 57-83
    • Gullion, T.1    Schaefer, J.2
  • 37
    • 0000844732 scopus 로고    scopus 로고
    • Introduction to rotational-echo, double-resonance NMR
    • Gullion T. Introduction to rotational-echo, double-resonance NMR. Concepts Magn. Reson. 10:1998;277-289.
    • (1998) Concepts Magn. Reson. , vol.10 , pp. 277-289
    • Gullion, T.1
  • 38
    • 0000165556 scopus 로고
    • DANTE-Z - A new approach for accurate frequency-selectivity using hard pulses
    • Boudot D., Canet D., Brondeau J., Boubel J.C. DANTE-Z - a new approach for accurate frequency-selectivity using hard pulses. J. Magn. Reson. 83:1989;428-439.
    • (1989) J. Magn. Reson. , vol.83 , pp. 428-439
    • Boudot, D.1    Canet, D.2    Brondeau, J.3    Boubel, J.C.4
  • 39
    • 0000414471 scopus 로고
    • Transferred-echo double-resonance NMR
    • Hing A.W., Vega S., Schaefer J. Transferred-echo double-resonance NMR. J. Magn. Reson. 96:1992;205-209.
    • (1992) J. Magn. Reson. , vol.96 , pp. 205-209
    • Hing, A.W.1    Vega, S.2    Schaefer, J.3
  • 40
    • 0033208603 scopus 로고    scopus 로고
    • 13C multiple-quantum correlation in solids under ultra-fast MAS
    • 13C multiple-quantum correlation in solids under ultra-fast MAS. J. Magn. Reson. 140:1999;471-476.
    • (1999) J. Magn. Reson. , vol.140 , pp. 471-476
    • Saalwächter, K.1    Graf, R.2    Spiess, H.W.3
  • 42
    • 0035307855 scopus 로고    scopus 로고
    • 13C multiple-spin correlation in solid-state NMR: Combining REDOR recoupling and multiple-quantum spectroscopy
    • 13C multiple-spin correlation in solid-state NMR: combining REDOR recoupling and multiple-quantum spectroscopy. J. Chem. Phys. 114:2001;5707-5728.
    • (2001) J. Chem. Phys. , vol.114 , pp. 5707-5728
    • Saalwächter, K.1    Spiess, H.W.2
  • 43
    • 0033629934 scopus 로고    scopus 로고
    • Sensitivity enhancement in solid state N-15 NMR by indirect detection with high-speed magic angle spinning
    • Ishii Y., Tycko R. Sensitivity enhancement in solid state N-15 NMR by indirect detection with high-speed magic angle spinning. J. Magn. Reson. 142:2000;199-204.
    • (2000) J. Magn. Reson. , vol.142 , pp. 199-204
    • Ishii, Y.1    Tycko, R.2
  • 44
    • 0034806939 scopus 로고    scopus 로고
    • Sensitivity enhancement in solid-state C-13 NMR of synthetic polymers and biopolymers by H-1 NMR detection with high-speed magic angle spinning
    • Ishii Y., Yesinowski J.P., Tycko R. Sensitivity enhancement in solid-state C-13 NMR of synthetic polymers and biopolymers by H-1 NMR detection with high-speed magic angle spinning. J. Am. Chem. Soc. 123:2001;2921-2922.
    • (2001) J. Am. Chem. Soc. , vol.123 , pp. 2921-2922
    • Ishii, Y.1    Yesinowski, J.P.2    Tycko, R.3
  • 46
    • 0037130635 scopus 로고    scopus 로고
    • 1H bond length determination in natural abundance by inverse detection in fast-MAS solid-state NMR spectroscopy
    • 1H bond length determination in natural abundance by inverse detection in fast-MAS solid-state NMR spectroscopy. J. Am. Chem. Soc. 124:2002;10938-10939.
    • (2002) J. Am. Chem. Soc. , vol.124 , pp. 10938-10939
    • Schnell, I.1    Saalwächter, K.2
  • 47
    • 0036708553 scopus 로고    scopus 로고
    • REDOR-based heteronuclear dipolar correlation experiments in multi-spin systems: Rotor-encoding, directing, and multiple distance and angle determination
    • Saalwächter K., Schnell I. REDOR-based heteronuclear dipolar correlation experiments in multi-spin systems: rotor-encoding, directing, and multiple distance and angle determination. Solid State Nucl. Magn. Reson. 22:2002;154-187.
    • (2002) Solid State Nucl. Magn. Reson. , vol.22 , pp. 154-187
    • Saalwächter, K.1    Schnell, I.2
  • 48
    • 0035542668 scopus 로고    scopus 로고
    • 1H NMR spectroscopy in the solid state: Very fast sample rotation and multiple-quantum coherences
    • 1H NMR spectroscopy in the solid state: very fast sample rotation and multiple-quantum coherences. J. Magn. Reson. 151:2001;153-227.
    • (2001) J. Magn. Reson. , vol.151 , pp. 153-227
    • Schnell, I.1    Spiess, H.W.2
  • 53
    • 0035542910 scopus 로고    scopus 로고
    • Advanced solid-state NMR methods for the elucidation of structure and dynamics of molecular, macromolecular, and supramolecular systems
    • Brown S.P., Spiess H.W. Advanced solid-state NMR methods for the elucidation of structure and dynamics of molecular, macromolecular, and supramolecular systems. Chem. Rev. 101:2001;4125-4155.
    • (2001) Chem. Rev. , vol.101 , pp. 4125-4155
    • Brown, S.P.1    Spiess, H.W.2
  • 55
    • 0034819067 scopus 로고    scopus 로고
    • Structure assignment in the solid state by the coupling of quantum chemical calculations with NMR experiments: A columnar hexabenzocoronene derivative
    • Ochsenfeld C., Brown S.P., Schnell I., Gauss J., Spiess H.W. Structure assignment in the solid state by the coupling of quantum chemical calculations with NMR experiments: a columnar hexabenzocoronene derivative. J. Am. Chem. Soc. 123:2001;2597-2606.
    • (2001) J. Am. Chem. Soc. , vol.123 , pp. 2597-2606
    • Ochsenfeld, C.1    Brown, S.P.2    Schnell, I.3    Gauss, J.4    Spiess, H.W.5
  • 56
    • 0035353543 scopus 로고    scopus 로고
    • Big is beautiful - 'Aromaticity' revisited from the viewpoint of macromolecular and supramolecular benzene chemistry
    • M.D. Watson, A. Fechtenkötter, K. Müllen, Big is beautiful - 'aromaticity' revisited from the viewpoint of macromolecular and supramolecular benzene chemistry, Chem. Rev. 101 1267-1300.
    • Chem. Rev. , vol.101 , pp. 1267-1300
    • Watson, M.D.1    Fechtenkötter, A.2    Müllen, K.3
  • 57
    • 0037183038 scopus 로고    scopus 로고
    • Structure and dynamics in columnar discotic materials: A combined X-ray and solid-state NMR study of hexabenzocoronene derivatives
    • Fischbach I., Pakula T., Minkin P., Fechtenkötter A., Müllen K., Spiess H.W., Saalwächter K. Structure and dynamics in columnar discotic materials: a combined X-ray and solid-state NMR study of hexabenzocoronene derivatives. J. Phys. Chem. B. 106:2002;6408-6418.
    • (2002) J. Phys. Chem. B , vol.106 , pp. 6408-6418
    • Fischbach, I.1    Pakula, T.2    Minkin, P.3    Fechtenkötter, A.4    Müllen, K.5    Spiess, H.W.6    Saalwächter, K.7
  • 59
    • 0037065186 scopus 로고    scopus 로고
    • C-3-symmetrical supramolecular architectures: Fibers and organic gels from discotic trisamides and trisureas
    • van Gorp J.J., Vekemans J.A.J.M., Meijer E.W. C-3-symmetrical supramolecular architectures: fibers and organic gels from discotic trisamides and trisureas. J. Am. Chem. Soc. 124:2002;14759-14769.
    • (2002) J. Am. Chem. Soc. , vol.124 , pp. 14759-14769
    • Van Gorp, J.J.1    Vekemans, J.A.J.M.2    Meijer, E.W.3


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